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INZEA F18P Blown Film/Cast Extrusion Biodegradable Polylactic Acid

    • Product Name: INZEA F18P Blown Film/Cast Extrusion Biodegradable Polylactic Acid
    • Factroy Site: Yudu County, Ganzhou, Jiangxi, China
    • Price Inquiry: admin@ascent-chem.com
    • Manufacturer: Ascent Petrochem Holdings Co., Limited
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    Specifications
    HS Code 412021
    Density 1.24-1.25 g/cm³
    Melt Flow Rate 190 C 2 16 Kg 4-8 g/10 min
    Melting Temperature 145-155 °C
    Glass Transition Temperature 55-60 °C
    Tensile Strength 25-35 MPa
    Elongation At Break 200-400%
    Tensile Modulus 600-1000 MPa
    Biobased Content >60%
    Biodegradability Yes
    Compostability EN 13432 compliant
    Food Contact Compliance Suitable for food contact
    Moisture Content <0.5%

    As an accredited INZEA F18P Blown Film/Cast Extrusion Biodegradable Polylactic Acid factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing INZEA F18P biodegradable polylactic acid resin supplied in 25 kg moisture-barrier paper bags, palletized for blown film and cast extrusion.
    Container Loading (20′ FCL) 20′ FCL loading of INZEA F18P biodegradable polylactic acid pellets: palletized, stretch-wrapped, approximately 18–20 MT net, for blown film/cast extrusion.
    Shipping INZEA F18P Blown Film/Cast Extrusion Biodegradable Polylactic Acid is shipped as solid pellets in sealed moisture-barrier bags, usually 25 kg sacks or bulk bags on pallets. It is typically non-hazardous for transport, requires no special dangerous goods classification, and should be stored cool, dry, and away from direct sunlight.
    Storage Store INZEA F18P in a cool, dry, well-ventilated warehouse, ideally below 30°C and below 50% relative humidity. Keep original packaging tightly closed, away from direct sunlight, heat, moisture, and ignition sources. Protect from humid air and UV exposure to prevent hydrolysis and degradation. Avoid strong acids, bases, oxidizers, and solvents. Use first-in, first-out rotation and observe recommended shelf life.
    Shelf Life Typically 12 months when stored unopened in original packaging, cool and dry, away from moisture, heat, and direct sunlight.
    Application of INZEA F18P Blown Film/Cast Extrusion Biodegradable Polylactic Acid

    Monolayer blown-film conversion of INZEA F18P for fresh-produce bags and checkout sacks starts from a moisture-control threshold rather than a temperature setpoint alone. Pre-drying in a desiccant-wheel dryer at 80°C for 4 h with supply-air dew point below -40°C is required to bring residual moisture below 250 ppm. Moisture levels above 400 ppm are reported to reduce mean molecular weight and produce edge fibrillation at the film tower. The extruder specification uses L/D 30:1 to 36:1 barrier screws with grooved feed sections and double-flight mixing elements. Melt temperature measured at the die is controlled between 185°C and 200°C. Die temperature is monitored in at least three zones; deviations beyond ±3°C across the circumference create gauge bands measurable by ISO 4591. Screen pack configuration 60/80/100 mesh protects the die and raises backpressure before a melt pump. The melt pump suction pressure setpoint is maintained within ±0.5 MPa of the extruder discharge to reduce surging. Die gap is set to 0.8–1.2 mm for monolayer film at 15–25 µm nominal thickness. Blow-up ratio is held between 2.5:1 and 3.5:1. Frost line height is fixed using chilled-air flow at 200–350 mm above the die face. Slip and antiblock masterbatch at 0.5–1.0 wt% is blended before the feed throat. Addition below 0.3 wt% leads to winder blocking on lines above 60 m/min; addition above 1.5 wt% depresses seal initiation and increases haze. Mechanical acceptance uses ISO 527-3:2018 for longitudinal and transverse tensile properties, ASTM D1709-16a method A for dart impact, and ASTM D1922 for Elmendorf tear. Compostability claims are checked against EN 13432:2000 with ≥90% biodegradation relative to cellulose under ISO 14855-1 within 180 days and ≥90% disintegration by dry mass after 12 weeks under controlled composting. In-line edge slitting has shown a tendency toward microcracking when die-lip temperature deviates more than ±4°C from setpoint; this behavior is consistent with the low melt strength of PLA homopolymer. Line reports from similar PLA monolayer lines indicate that start-up edge trim is higher than PE by a factor of two during the first 30 min of production and stabilizes below 5 wt% thereafter.

    What Drives Cast-Film Optical Degradation and Neck-In in Dry-Food Pouch Structures?

    Converted on a cast line for dry-food pouches, INZEA F18P presents a separate set of setpoints. The resin is pre-dried under the same 250 ppm moisture limit, but the melt temperature is shifted upward to 200–215°C to lower melt viscosity. Flat-die processing uses a die gap of 0.6–0.9 mm, an air gap of 10–25 mm, and a polished chill roll at 25–40°C. Neck-in is measured directly from die width to sheet width after quenching; converter reports indicate neck-in exceeding 10% at 20 mm air gap for 20 µm PLA cast film, higher than PP under comparable draw. Draw resonance appears when line speed exceeds 80 m/min at an air gap above 25 mm. Reducing the air gap to 10–15 mm moves the resonance threshold above 120 m/min on 20 µm film. Optical haze is measured by ASTM D1003-21. Haze is controlled by chill roll temperature and melt temperature. At chill roll temperatures above 40°C, the slow quench allows spherulite growth that raises haze beyond 5%. At melt temperatures above 215°C, lactide regeneration raises free-monomer content and can deposit oligomer on the chill roll face, producing release defects visible as repeating bands. Corona treatment at 42–46 dyn/cm is applied in-line before winding; the dyne level is verified by ASTM D2578-17. Food-contact compliance for dry food must be evaluated on the finished article under EU 10/2011 as amended, using food simulant E at 40°C for 10 days; overall migration must remain below 10 mg/dm². In the U.S. the finished pouch may fall under 21 CFR 175.300 if the cast film is used as a resinous coating on paper or board, or under a food contact notification for the base resin; the raw material certificate alone does not constitute clearance. This structure is not appropriate for high-moisture or high-fat products because PLA permeability and migration conditions require a full barrier assessment.

    Agricultural Mulch Film Fragmentation Windows and Soil Contact Thresholds Under EN 17033

    For agricultural mulch film, INZEA F18P is not processed as a neat resin. A typical soil-biodegradable mulch structure consists of 70–80 wt% INZEA F18P, 20–30 wt% PBAT, 2–5 wt% talc, and 0.2–0.5 wt% processing stabilizer masterbatch. PBAT is added to improve dart impact and tear propagation, but it narrows the thermal window. Melt blending on a twin-screw compounding line with L/D 40:1 and vent port at -0.08 MPa is followed by pelletizing under water cooling. The blown-film line uses a L/D 30:1 single-screw extruder with a Maddock mixing section. Melt temperature at the die is controlled between 170°C and 180°C. Below 170°C the PLA phase shows poor homogenization; above 185°C PBAT begins to release volatile degradation products and pressure fluctuation increases. The usable window of ±5°C is maintained by three-zone die heaters and a melt pump with closed-loop pressure control. Die gap is 1.0–1.4 mm. Blow-up ratio is 2.0:1–2.8:1. Frost line height is 400–700 mm to allow the blend to stabilize; too low a frost line creates MD orientation that later causes premature fragmentation along planting rows. Finished thickness is 12–15 µm for seasonal vegetable crops. Tensile tests after conditioning at 23°C/50% RH for 48 h are performed under EN ISO 527-3:2018. Tear resistance is measured under ISO 6383-2. Accelerated weathering is not the same as soil degradation; a mulch film may show mechanical embrittlement under UV after 200–300 h in ISO 4892-2 while still requiring soil biodegradation under EN 17033:2018. EN 17033 requires ≥90% soil biodegradation within 24 months under ISO 17556, non-negative ecotoxicity results, and metal content limits. Published data for F18P-specific soil half-life under European field conditions is limited; converters must validate against local soil type and temperature. On a 75 mm screw blown-film line, reducing PBAT from 30 wt% to 20 wt% at constant output raises specific energy and screw torque by approximately 10–20%, and edge instability increases below 20 wt% PBAT. This operational boundary is the reason the blend ratio is not used as a cost lever on production lines.

    Converting platformPre-drying targetMelt temperatureDie gapDimensional controlInstability threshold
    Monolayer blown film250 ppm185–200°C0.8–1.2 mmBUR 2.5:1–3.5:1, frost line 200–350 mmEdge slitting microcracks beyond ±4°C die-lip deviation
    PBAT blend blown film250 ppm before compounding170–180°C1.0–1.4 mmBUR 2.0:1–2.8:1, frost line 400–700 mmVolatile degradation and pressure fluctuation above 185°C
    Cast film and coating250 ppm before extrusion200–215°C0.5–0.9 mmAir gap 10–180 mm, chill roll 15–40°CDraw resonance above 80–120 m/min depending on air gap

    During paperboard coating for cold-beverage cups and sandwich wedges, INZEA F18P is restricted to short-contact moisture conditions. The cast coater uses a L/D 30:1 extruder, deckled flat die with 0.5 mm gap, air gap 120–180 mm, and matte chill roll at 15–25°C. Coating weight is held at 20–40 g/m² by gravimetric control. Paperboard is corona-treated to 38–42 dyn/cm immediately before the nip. Mechanical adhesion is adequate for coating weights above 30 g/m²; below that level, surface polarity mismatch and the rapid quench of PLA reduce bond strength. Draw resonance is the primary speed constraint. At an air gap of 180 mm, line speed is kept below 100 m/min to avoid periodic thickness bands. The coated board is tested for overall migration under EU 10/2011 with dry-food simulant conditions at 40°C for 10 days. The PLA layer is not a gas barrier. Water vapour transmission rate of monolayer PLA is generally above 200 g/m²·day at 25 µm under 38°C/90% RH when measured by ISO 15106-3; published data for this specific INZEA grade in this configuration is limited. Applications requiring shelf-stable moisture protection therefore require an additional barrier substrate or laminated film, not the PLA layer alone.

    When Mailer Film Perimeter Seal Integrity Shifts Below 30 µm

    Compostable e-commerce mailer sleeves can be produced from INZEA F18P on a monolayer blown-film line when thickness is kept between 30 µm and 50 µm. The primary quality issue is perimeter seal integrity after printing and converting. Heat sealing is performed at 120–140°C jaw temperature, 0.2–0.5 MPa pressure, and 0.5–1.5 s dwell. Seal strength is measured according to ASTM F88/F88M-21. Acceptance is typically set not below 6 N/15 mm for mailers of 40 µm. At thickness below 30 µm, the seal window narrows because the film web loses heat to the jaw surface rapidly. Seal strength drops below 4 N/15 mm when jaw temperature is 5°C below the lower limit. On high-speed lines with gusseted side seals, seal initiation temperature rises by 8–12°C when the printed ink layer is on the sealant side. This is controlled by leaving a seal band free of ink or by changing the seal jaw profile. Puncture resistance is measured by ASTM D5748 or EN 14477 depending on the customer specification. A biodegradable flexibilizer masterbatch at 2–4 wt% is added to improve puncture and flex crack resistance. Above 6 wt%, the film becomes difficult to slit and the coefficient of friction rises above 0.6. Compostability claims for the complete mailer with adhesive label and paper insert must be verified as a finished article under EN 13432:2000 or ASTM D6400. Standard practice requires testing the worst-case adhesive concentration. A label area above 15% of the mailer surface can dominate disintegration results because the adhesive may remain as a hot-melt residue in the compost.

    Compostable Bin Liner Tear Resistance and Dart Impact Variability in High-BUR Operation

    In organic waste collection, compostable bin liners produced from INZEA F18P require film gauges of 18–30 µm and high resistance to point puncture from bones and stems. INZEA F18P is run on a triple-layer blown-film die either in all layers or with a PBAT-rich skin layer. The use of a PBAT-rich skin layer at 20 wt% of total thickness improves dart impact by 15–25% relative to a monolayer at the same gauge, based on comparative line evaluations using ASTM D1709-16a. The skin layer is achieved with separate extruders feeding the outer layers. The core can contain 15–25 wt% reclaimed trim from edge slitting. Regrind must be pre-dried to below 250 ppm moisture before reintroduction. High blow-up ratios of 3.0:1–4.0:1 increase transverse tear and dart impact but reduce machine-direction tensile yield. At BUR above 4.0:1, the film shows bubble instability and diameter oscillation on a 200 mm die unless a cooled internal bubble stabilizer is active. The frost line is held at 250–450 mm. Elmendorf tear is measured by ASTM D1922. The transverse tear value commonly exceeds the machine-direction value by 20–40% in high-BUR operation. Seal and dart acceptance follow the customer specification; dart impact is thickness-dependent and is reported by ASTM D1709-16a method A or B. At 18 µm, the dart impact of neat INZEA F18P is insufficient for load-bearing organic waste sacks. PBAT blending of 10–20 wt% or a three-layer structure with PBAT skins is required. Published data for the exact F18P monolayer dart impact at 18 µm is limited. Compostability compliance for bin liners is typically evaluated under EN 13432:2000 or ASTM D6400. The organic waste collection bag must also satisfy local certification rules, which may require home-compostability testing under AS 5810 or NF T51-800 depending on export market.

    CriterionStandard or methodNumeric thresholdPractical boundary
    Industrial compostability, EUEN 13432:2000 + ISO 14855-1≥90% biodegradation in 180 days; ≥90% disintegration in 12 weeksFinished article including inks and adhesives must be tested
    Industrial compostability, USASTM D6400≥90% biodegradation; ≥90% disintegrationAerobic composting conditions apply
    Soil biodegradable mulchEN 17033:2018 + ISO 17556≥90% biodegradation in 24 monthsEcotoxicity and metal content limits are mandatory
    Dry-food overall migrationEU 10/2011<10 mg/dm²Simulant E, 40°C, 10 days
    Mailer seal strengthASTM F88/F88M-21≥6 N/15 mm at 40 µmProcess acceptance value, not a legal limit
    Puncture propagationASTM D5748Thickness-dependentReported as propagation tear
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    Certification & Compliance
    More Introduction

    INZEA F18P is a polylactic acid (PLA)-based biodegradable thermoplastic compound specified for blown film and cast extrusion. The grade is supplied as pellets and is intended for conversion into monolayer and multilayer films in which industrial compostability, controlled optical clarity, and renewable carbon content are required. Because the resin is PLA-based, its melt rheology and moisture sensitivity differ markedly from polyethylene and PBAT-rich compounds; the processing envelope is narrower and requires defined drying, extrusion, and bubble-cooling parameters to avoid hydrolysis, lactide regeneration, and gel formation. The grade is generally assessed for compostability under EN 13432:2000, ASTM D6400-19, or ISO 17088:2021; certification of the final film depends on thickness, printing, lamination, and additive loading. The following paragraphs set out the technical boundaries relevant to the model, including comparison with other biodegradable film resins and standard test methods applicable to finished film property verification.

    How Are Drying and Melt-Temperature Limits Managed During Extrusion of INZEA F18P?

    Moisture control is the first critical variable. Polylactic acid undergoes hydrolytic chain scission during processing when moisture content exceeds 250 ppm; moisture uptake from ambient air can raise pellet moisture above 0.1 wt% within 4 h at 23 °C and 50% RH. A closed-loop desiccant dryer with a supply air dew point of -40 °C to -30 °C, a hopper setpoint of 80 °C ± 5 °C, and a residence time of 4 h to 6 h is therefore required. The dried pellets should be transferred by vacuum or dry-air conveying to the extruder throat; if ambient humidity exceeds 60% RH, the hopper should be blanketed with dried air or nitrogen. Monitoring by ISO 15512:2019 or an equivalent Karl Fischer method is recommended before first production and after any line stoppage longer than 15 min.

    Barrel temperatures should start at 160 °C to 165 °C in the feed section and rise to 175 °C to 185 °C in the metering section. Adapter and die zones are normally set at 180 °C to 195 °C, with the measured melt temperature at the die maintained below 200 °C. Above 210 °C, lactide regeneration and non-linear viscosity loss accelerate, producing acrid odour, yellowing, and gel defects; below 175 °C, melt fracture and film gel streaks can develop. The practical melt-temperature window is therefore approximately ±5 °C around a line-specific optimum. Screw speed should be balanced with output to keep residence time below 8 min, preferably 4 min to 6 min, and melt pressure at the die should remain below 250 bar for spiral mandrel dies; pressures above 300 bar indicate screen-pack plugging or insufficient melt temperature. A breaker plate with 60/80/120 mesh screen pack is commonly used at start-up; a 100 mesh final screen can be retained if pressure permits.

    Extruder configuration influences degradation. A single-screw extruder with a grooved feed section, 25 L/D to 30 L/D, and a barrier screw with a compression ratio of 2.5:1 to 3.5:1 is preferred over high-shear compounding screws. Twin-screw compounding is not required for direct film conversion and may over-shear the melt unless downstream melt cooling is applied. The use of static mixers or melt pumps is acceptable only if residence time remains controlled. Corrosion-resistant screw and barrel surfaces are not mandatory for neat PLA, but flame-hardened or nitrided barrels reduce wear when the grade is blended with mineral fillers.

    Blown film operation on conventional polyethylene lines requires a die gap of 0.8 mm to 1.2 mm, a blow-up ratio of 2.0:1 to 3.5:1, and a frost-line height between 1.5 and 4.0 die diameters. Use of a dual-lip air ring with chilled air at 10 °C to 20 °C improves bubble stability and prevents blocking; internal bubble cooling is beneficial above 80 kg/h output. Gauge variation should be maintained below ±5% for certification-grade film. Corona treatment at 1.5 kW to 3 kW per meter of web width and 10 m/min to 30 m/min line speed is used to raise surface energy above 38 mN/m for water-based ink adhesion. Winding tension should be reduced compared with polyethylene because the film surface tends to block; a maximum winding taper tension of 0.2 N/mm is recommended.

    For cast extrusion, the die gap is normally set at 0.4 mm to 0.6 mm for a 0.3 mm slot die, with an air gap of 10 mm to 30 mm. Chill roll temperatures from 20 °C to 40 °C are used to reduce crystallinity and increase optical clarity. Vacuum box or electrostatic pinning improves web contact. Line speeds up to 250 m/min are possible with cast film, but edge trim should be maintained below 15% of total web width to avoid excessive scrap from neck-in.

    Comparative Mechanical and Regulatory Position Against Other Film Grades

    The product differs from high-flow PLA injection-moulding grades in melt-flow rate and melt strength. High-flow PLA typically falls between 15 g/10 min and 30 g/10 min at 190 °C/2.16 kg under ISO 1133-1:2022, whereas INZEA F18P is formulated for film extrusion and is normally below 10 g/10 min, with most published data in the 3 g/10 min to 7 g/10 min range. The resulting melt strength supports a stable blown film bubble but reduces injection moulding flow length, making F18P unsuitable for thin-wall injection moulding. In comparison with PBAT-rich PLA compounds, F18P has a higher renewable carbon fraction and higher stiffness, but lower tear resistance and dart impact. Converters replacing a PBAT-rich compound with F18P should evaluate tear resistance under ISO 6383-2:1983 and dart impact under ASTM D1709-22 at the same film gauge, and should increase gauge by 20% to 40% if equivalent toughness is required.

    Mechanical property ranges for blown F18P films at 25 µm gauge are typically: tensile strength at break between 35 MPa and 50 MPa in machine direction and 20 MPa to 35 MPa in transverse direction; elongation at break between 100% and 250% in machine direction and 80% to 180% in transverse direction; dart impact by ASTM D1709-22 Method A between 80 g and 150 g; tear resistance by ISO 6383-2:1983 between 150 mN and 300 mN. These values are strongly dependent on blow-up ratio, frost-line position, and degree of orientation; they are not conversion guarantees.

    Barrier properties are moderate. Oxygen transmission rate for a 25 µm blown film at 23 °C and 0% RH is often stated in the range of 500 cm³/(m²·day·atm) to 800 cm³/(m²·day·atm) under ASTM D3985-17, and water vapour transmission rate at 38 °C and 90% RH ranges from 300 g/(m²·day) to 500 g/(m²·day) under ASTM F1249-20. These values place INZEA F18P films between polyolefins and high-barrier biodegradable polyesters, making them suitable for breathable packaging but not for high-barrier applications without additional layers or coatings.

    Standard Measurement focus Typical requirement
    EN 13432:2000 Industrial compostability, heavy metals, disintegration, ecotoxicity 90% biodegradation in 180 days; ≥90% disintegration in 12 weeks
    ASTM D6400-19 Plastics labelled as compostable in municipal or industrial facilities 90% carbon conversion to CO₂ in 180 days; 90% disintegration in 12 weeks
    ISO 17088:2021 Compostable plastics specification Biodegradation, disintegration, ecotoxicity and heavy-metal limits
    ISO 16929 Pilot-scale aerobic disintegration 90% after 12 weeks
    REACH SDS and SVHC compliance Confirm current SDS for each final article

    Operational boundaries are explicit. The resin should not be processed at melt temperatures above 210 °C or at high shear rates for extended periods. It should not be combined with amine-based additives, some calcium or zinc stearates, or acidic or basic masterbatches, because such additives can catalyse ester hydrolysis and reduce molecular weight. Blends with PVC or EVOH are not recommended unless a dedicated tie layer is used and the line is purged with a PLA-compatible purging compound. Storage should be in sealed, foil-lined containers or dry-air silos; once opened, pellets should be used within 24 h if ambient relative humidity exceeds 60%. Processing equipment should be purged with a low-viscosity PLA or polyolefin purge grade before shutdown; leaving PLA in the barrel at elevated temperature for more than 15 min can produce carbonised deposits and block the die.

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