| HS Code | 321048 |
| Material Type | Polylactic Acid (PLA) |
| Density | 1.24 g/cm³ |
| Melt Flow Rate | 20 g/10 min (210°C/2.16 kg) |
| Crystalline Melt Temperature | 165°C |
| Glass Transition Temperature | 55-60°C |
| Tensile Strength | 50 MPa |
| Tensile Elongation At Break | 10% |
| Tensile Modulus | 3.5 GPa |
| Flexural Modulus | 3.5 GPa |
| Notched Izod Impact Strength | 20 J/m |
| Vicat Softening Point | 55°C |
| Heat Deflection Temperature | 55°C (0.45 MPa) |
| Moisture Content | <0.025% |
As an accredited Ingeo™ Biopolymer 6752D Staple Fiber-Grade PLA factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.
| Packing | Ingeo™ Biopolymer 6752D Staple Fiber-Grade PLA is supplied in 25 kg (55 lb) polyethylene-lined multiwall bags, palletized and shrink-wrapped. |
| Container Loading (20′ FCL) | 20′ FCL: 20 pallets, 40 × 25 kg bags each, total 20,000 kg Ingeo™ Biopolymer 6752D Staple Fiber-Grade PLA, shrink-wrapped. |
| Shipping | Ingeo™ Biopolymer 6752D Staple Fiber-Grade PLA is shipped as non-hazardous, non-regulated solid pellets. No UN number, hazard class, or packing group applies. It is typically packaged in moisture-barrier bags or bulk containers. Store dry, away from heat, and transport according to local regulations. |
| Storage | Store Ingeo™ Biopolymer 6752D Staple Fiber-Grade PLA in a cool, dry, well-ventilated area, away from direct sunlight, heat, ignition sources, and moisture. Keep original packaging tightly sealed to prevent hydrolysis. Maintain stable temperatures, ideally below 30°C, with low relative humidity. Avoid prolonged humid or hot storage; use stock first-in, first-out. |
| Shelf Life | Ingeo 6752D PLA has a 12-month shelf life when stored unopened, dry, below 50°C, and protected from direct sunlight. |
On high-speed spunlace lines with 2.8–3.2 m working width and 90–120 m/min delivery speed, Ingeo™ Biopolymer 6752D staple fibre is opened as the synthetic component of an industrial wipe web at a fibre mass fraction of 30–70 wt%, the balance being viscose or lyocell stock with a finished web basis weight of 35–85 g/m². The 6752D staple is specified at 1.7–3.3 dtex linear density and 38–51 mm cut length; the lower-denier range is assigned to facial and glass-cleaning substrates, while the upper-denier range is retained for heavy-duty industrial wipes. The carded web is cross-lapped to target weight and hydroentangled at first-stage water pressure of 40–110 bar and second-stage pressure of 120–180 bar, followed by through-air drying at a maximum fabric temperature of 105 °C. The controlling test protocols are ISO 9073-3 for tensile strength, ISO 9073-6 for absorbent capacity, EDANA/INDA NWSP 010.3.R0 for web uniformity, and OECD 301B where ready biodegradability is to be claimed. If ambient bale-storage relative humidity exceeds 60%, the fibre must be conditioned to 45–55% RH before opening; otherwise moisture uptake lowers fibre stiffness and reduces hydroentanglement energy transfer at the same pressure settings. Terminal finished products include dry industrial surface-cleaning cloths, pre-moistened biobased cleaning wipes, and food-service wipe substrates requiring FDA 21 CFR 177.1520 verification where no functional barrier separates the fibre from food-contact surfaces.
Mill data from three-cards-and-one-lapper lines running at 90–130 m/min indicate that 6752D addition above 25 wt% narrows the thermal bonding window because the PLA fibre begins to soften before the polyethylene sheath reaches full flow. In disposable hygiene acquisition/distribution layers, 6752D is introduced at 15–25 wt% with a bicomponent PE/PET sheath-core fibre at 75–85 wt%; the PE sheath melting point is 125–135 °C and the PLA fibre surface must remain dimensionally stable below 155 °C. The blended staple is carded at 18–24 m/min cylinder surface speed, cross-lapped to 45–80 g/m², and thermally bonded in a through-air oven at 138–142 °C with a residence time of 2.5–4.0 s. Downstream embossed calender bonding operates at nip pressures of 0.4–0.6 MPa and roll temperatures of 140–148 °C; excursions beyond 155 °C produce PLA film deposition on the engraved roll and increase web-break frequency on high-speed converting lines. The test protocol stack comprises ISO 9073-8 for liquid strike-through time, EDANA/INDA NWSP 070.3.R0 for multiple-strike-through performance, ISO 9073-6 for absorption capacity, and EDANA/INDA NWSP 120.6.R0 for absorbency under load. Terminal product types are acquisition layers for infant diapers, feminine-care transfer layers, and adult incontinence acquisition layers.
Where door panel scrim and trunk liner backings must satisfy VDA 278:2011-10 volatile organic compound and fogging limits, 6752D staple is needled into recycled polyester at a blend ratio of 30–45 wt% 6752D, 40–50 wt% rPET, and 10–25 wt% low-melt co-PET bicomponent fibre. The carded web is cross-lapped to 300–900 g/m² and needlepunched at 250–400 punches/cm² on a standard double-board needle loom, followed by thermal stabilisation at 145 °C for 90 s and rotary die cutting. Flammability acceptance is tested to ISO 3795 and FMVSS 302, with the typical burn rate for a 600 g/m² needlepunch containing 40 wt% 6752D held below 100 mm/min; colour-change assessment after heat ageing is performed to ISO 105-A02. The operational boundary is set by needlepunch tear strength: above 45 wt% 6752D, lower fibre-to-fibre friction reduces z-direction entanglement and lowers trapezoidal tear resistance, so wheel arch liner and trunk side-trim formulations cap the PLA fraction at 40 wt%. Terminal products include door panel scrim, parcel shelf backing, trunk lining, and wheel arch acoustic liners.
In carded pre-filter mats, 6752D staple contributes a lofted void volume that is progressively reduced by needling; the fibre is positioned at 20–35 wt% with the balance being 65–80 wt% polyethylene terephthalate or bicomponent PET/co-PET carrier fibre. The process begins with carding at 15–20 m/min output speed, cross-lapping to 150–300 g/m², and needlepunching at 200–350 punches/cm²; after needling the mat is pleated at a maximum blade and roller temperature of 70 °C because PLA thermal memory can reduce pleat sharpness above that threshold. The relevant classification standard is ISO 16890-1 for particulate matter efficiency, supported by ASHRAE 52.2 arrestance testing; the typical positioning is an ePM10 pre-filter rather than an ePM1 or ePM2.5 primary filter. Pressure-drop acceptance is examined under ISO 29462 field-performance protocols, and fibre shedding is limited by the needlepunch density ceiling because excessive punching fractures the PLA staple and creates measurable particulate carryover. Published data for 6752D in classified high-efficiency final filters is limited; therefore the fibre is specified only in pre-filter layers and paint-booth exhaust mats. Terminal product types include HVAC panel pre-filters, paint-spray booth dry-filter panels, and low-temperature cabin air pre-filters.
Duvet and outdoor insulation wadding lines running at 45–60 m/min deliver 6752D at a fibre mass fraction of 50–100 wt%, with the remaining 0–50 wt% being recycled PET hollow staple or a low-melt bicomponent binder fibre added at 10–20 wt% of total web mass when loft retention above 85% is required after compression cycling. The garnett web is cross-lapped to 1,200–2,400 g/m² and through-air bonded at 130–160 °C depending on the binder sheath melt point; the final batt is slit and compressed into rollstock or die-cut inserts. Thermal resistance is quantified under ISO 5085-1, flammability under EN ISO 12952-1, and fibre blend proportion under ISO 1833-1; the finished batt must also meet OEKO-TEX Standard 100 Annex 4 classification when marketed for infant or direct-skin textile applications. The operational limitation is sustained service temperature: continuous exposure above 45 °C causes progressive dimensional relaxation and loft loss, so the wadding is not specified for heated bedding or tumble-drying above 60 °C exhaust temperature. Terminal product types include duvet inserts, pillow fills, mattress topper pads, and needle-punched insulation mid-layers for outerwear jackets.
A 30/70 or 50/50 6752D/combed cotton ring-spun yarn is developed on conventional blowroom and carding equipment, with the 6752D staple cut to 38 mm to align with cotton fibre length distribution and a fibre linear density of 1.7 dtex. The sliver is drawn to 0.5–0.8 ktex, roved, and ring-spun at 16,000–18,000 rpm spindle speed, with twist levels adjusted between 700–1,100 twists per metre to control hairiness without embrittling the PLA component. Yarn tensile acceptance is measured to ISO 2062 and ASTM D2256/D2256M, colourfastness to water to ISO 105-E01, and restricted substances to OEKO-TEX Standard 100 Annex 4. In wet processing, the dyebath temperature is held below 60 °C and the pH is maintained between 4.0 and 7.0 because alkaline conditions above pH 8 and elevated liquor temperature accelerate hydrolysis of the PLA fraction. The subsequent fabric is knitted on a 24-gauge single-jersey circular machine with cylinder speed of 28–32 rpm, producing a finished fabric weight of 120–220 g/m² after open-width finishing. Terminal product types include single-jersey base-layer garments, intimate apparel, leisurewear, and lightweight home-textile goods such as pillow ticking and mattress-ticking knit shells.
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Ingeo™ Biopolymer 6752D Staple Fiber-Grade PLA is a melt-spinnable polylactic acid resin supplied by NatureWorks LLC for conversion on conventional staple fiber lines producing cut staple, crimped tow, and cardable nonwoven feedstocks. The grade is a poly(L-lactic acid)-rich copolymer with a D-isomer content controlled near 4 mol% to balance crystallization rate and melt processability. Typical lot release data supplied by the manufacturer include density of 1.24 g/cm³ (ASTM D792), melt flow rate in the range of 14–16 g/10 min at 210 °C/2.16 kg (ASTM D1238), and a melting peak between 150 °C and 165 °C (ASTM D3418). The resin is differentiated from high-D amorphous PLA packaging grades by its capacity for strain-induced crystallization during fiber drawing, which permits heat-setting, crimp retention, and controlled low-shrinkage staple production.
Processing of 6752D on production-scale staple fiber lines begins with resin drying in desiccant dryers capable of maintaining dew point below -40 °C. Hydrolysis at the ester linkage is the dominant degradation mechanism; pellet moisture above 0.025 wt% (ASTM D6869) produces measurable pressure fluctuation, melt viscosity reduction, and oligomer bloom at spinneret surfaces. Single-screw extruders with L/D ratios from 24:1 to 30:1, compression ratios from 2.5:1 to 3.0:1, and barrel set points between 200 °C and 230 °C are typical for this grade on staple lines. Melt temperature should not exceed 250 °C because thermal depolymerization and acetaldehyde generation become kinetically significant above that threshold. Quench air temperature between 20 °C and 45 °C with relative humidity below 70% stabilizes amorphous orientation before drawing.
Drawing and heat-setting are critical differentiators. Staple fibers produced from 6752D are typically drawn to a total draw ratio between 2.8:1 and 4.0:1 to induce strain-induced crystallization; post-draw heat-setting in the range of 110 °C to 130 °C under tension is used to increase crystallinity and reduce hot-air shrinkage. Fiber tensile properties measured according to ISO 5079 commonly fall between 2.5 cN/dtex and 4.0 cN/dtex tenacity and 25% to 50% elongation at break, depending on draw ratio and quench homogeneity. Published data for this specific grade in needlepunch constructions are limited; therefore, exact carding-induced strength loss should be established through pilot trials.
Open storage at relative humidity above 60% is an operational boundary. Pellets exposed to ambient air for more than 4 h should be re-dried to the target moisture before entering the extruder. Regrind from spin line waste is not recommended unless it is collected dry, blended below 20 wt%, and re-dried under the same conditions; higher regrind fractions reduce melt strength and shift the draw resonance point.
The controlled resin parameters for 6752D as reported in manufacturer technical literature are presented in Table 1. Users should confirm lot-specific certificates of analysis before setting process control limits.
| Property | Test Method | Typical Controlled Range |
|---|---|---|
| Melt flow rate | ISO 1133-1 / ASTM D1238 | 14–16 g/10 min at 210 °C/2.16 kg |
| Density | ISO 1183-1 / ASTM D792 | 1.24 g/cm³ |
| Melting peak | ISO 11357-1 / ASTM D3418 | 150–165 °C |
| Glass transition | ISO 11357-2 / ASTM D3418 | 55–60 °C |
| D-lactide content | Manufacturer-controlled hydrolytic chiral analysis | approximately 4 mol% |
| Pellet moisture after drying | ISO 15512 / ASTM D6869 | <0.025 wt% |
Relative to high-D amorphous PLA packaging grades with D-isomer contents above 12 mol%, 6752D displays faster crystallization kinetics and a higher maximum achievable crystallinity, which are necessary for heat-set staple fiber dimensional stability. Compared with continuous filament PLA grades, 6752D is tuned for crimped staple production rather than high-speed partially oriented yarn take-up. Compared with polyolefin staple grades, 6752D requires more aggressive moisture management and lower melt temperatures; however, its density of 1.24 g/cm³ and biobased carbon content as measured by ASTM D6866 differentiate it in nonwoven and fiberfill applications where material-specific end-of-life claims are controlled by article certifications such as EN 13432 or ASTM D6400.
For staple fiber processes, the resin is extruded through spinnerets with hole counts from 500 to 3000, quenched, drawn, crimped, cut, and baled. Carding on high-speed nonwoven cards running above 120 m/min demands consistent crimp frequency and low fly; PLA staple has lower heat of fusion than PET, reducing calendar energy input but narrowing the bonding window. Thermal bonding in through-air or calendar units at roll temperatures between 120 °C and 150 °C is typical, but published data for this specific configuration is limited and must be optimized against line speed and basis weight. Basis weight should be measured according to ISO 9073-1 and cross-direction tensile strength according to ISO 9073-3 before release of commercial nonwoven specifications.
Spin finish selection is downstream but process-critical. Because PLA has low moisture regain, static dissipation on high-speed cards is controlled by antistatic finishes, not by resin moisture. Finish application levels between 0.2% and 0.6% by fiber weight are typical in carded nonwovens; excessive finish alters carding friction, while insufficient finish increases fly and cylinder loading. Needlepunch nonwovens produced at mass per unit area between 80 g/m² and 250 g/m² (ISO 9073-1) are common conversion targets for this grade.
In melt-spun PLA fiber, the D-isomer content is the primary molecular controller of crystal nucleation and growth. At approximately 4 mol% D-isomer, 6752D retains enough stereo-regularity for rapid strain-induced crystallization during drawing while avoiding excessive spherulitic crystallization in the quench chamber. Differential scanning calorimetry under a heating rate of 10 °C/min (ASTM D3418) commonly shows a cold crystallization exotherm between 90 °C and 120 °C and a melting endotherm between 150 °C and 165 °C. The position and area of the cold crystallization peak are sensitive to quench rate, draw ratio, and heat-setting temperature. Batch-to-batch shifts in D-isomer content within the manufacturer’s control range can alter crystallization half-time by seconds to minutes; therefore, downstream drawing and heat-setting recipes should be re-validated when lot changes occur.
The melt flow rate of 14–16 g/10 min at 210 °C/2.16 kg places 6752D in the low-viscosity fiber spinning envelope. PLA melt viscosity is shear-thinning and temperature-sensitive; spin pack pressure drop and die swell are therefore controlled by melt pump output and spinneret capillary geometry, not by raising melt temperature beyond the degradation threshold. On lines equipped with melt pumps, pressure deviations commonly indicate screen pack fouling or incorrect melt temperature rather than resin dryness after the extrusion zone.
Compliance status for finished articles produced from 6752D is summarized in Table 2. Resin supply does not itself constitute finished article certification.
| Standard or Regulation | Scope | Applicability to 6752D |
|---|---|---|
| EN 13432 | Compostable packaging recovery | Applies to finished article; certification required on final construction |
| ASTM D6400 | Compostable plastics in municipal or industrial composting | Finished article certification |
| ASTM D6866 | Biobased carbon content | Resin or article measurement; manufacturer lot data controls claim |
| ISO 14040 / ISO 14044 | Life cycle assessment framework | System-level study; not a product certification |
| REACH Regulation (EC) No 1907/2006 | Substance registration and authorization | Substance registration applies; downstream article obligations remain |
| EU Regulation 10/2011 | Food contact plastics | Finished article compliance; migration testing required per article |
Grade-specific published fracture and carding data for this exact resin in multi-layer nonwoven configurations remain sparse. Process qualification on target manufacturing lines is therefore required to establish article-level performance under ISO 9073 and ISO 5079 test conditions.