| HS Code | 941278 |
| Product Name | Ingeo™ Biopolymer 6060D Amorphous Fiber-Grade Staple Fiber PLA |
| Polymer Type | Polylactic Acid (PLA) |
| Grade | Amorphous Fiber-Grade Staple Fiber |
| Form | Pellets |
| Density | 1.24 g/cm³ |
| Melt Flow Rate | 15 g/10 min at 210°C/2.16 kg |
| Glass Transition Temperature | 55-60°C |
| Crystalline Melt Temperature | 155-170°C |
| Tensile Strength | 50 MPa |
| Tensile Modulus | 3.5 GPa |
| Elongation At Break | 3% |
| Flexural Modulus | 3.5 GPa |
| Notched Izod Impact | 2.5 kJ/m² |
| Vicat Softening Point | 60°C |
| Processing Temperature | 200-230°C |
| Drying Temperature | 80°C |
| Drying Time | 4 hours |
| Moisture Content | <0.025% |
| Biobased Content | 100% |
| Compostability | Industrial compostable per EN 13432 and ASTM D6400 |
As an accredited Ingeo™ Biopolymer 6060D Amorphous Fiber-Grade Staple Fiber PLA factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.
| Packing | Ingeo™ Biopolymer 6060D is supplied in 25 kg multiwall paper bags or 1,000 kg bulk bags, palletized for transport. |
| Container Loading (20′ FCL) | Loaded into 20-foot FCL containers; Ingeo™ Biopolymer 6060D Amorphous Fiber-Grade Staple Fiber PLA is palletized, shrink-wrapped, and secured for transport. |
| Shipping | Ingeo™ Biopolymer 6060D is shipped as solid PLA resin or staple fiber in moisture-barrier bags, totes, or bulk containers. It is non-hazardous, not DOT/IMDG/IATA regulated, with no UN number. Store dry, cool, away from moisture/UV. Use standard industrial hygiene; avoid dust. No special transport labels required. |
| Storage | Store Ingeo™ Biopolymer 6060D in a cool, dry, well-ventilated area at ambient temperature, away from heat, ignition sources, and direct sunlight. Keep containers tightly closed to prevent moisture uptake. Protect from temperatures above 50°C and humid conditions. Avoid physical damage; use first-in, first-out stock rotation. Do not stack excessively. Follow local regulations and manufacturer guidance. |
| Shelf Life | Shelf life is 12 months from manufacture when stored unopened in original packaging, cool and dry, below 50°C, away from moisture. |
In airlaid absorbent core manufacture for adult incontinence and feminine hygiene pads, 6060D amorphous PLA staple is introduced as a latex-free thermal binder at addition levels from 12 wt% to 18 wt% on dry furnish mass. The fluff pulp furnish is defibrated in a hammer mill to reduce node content, then blended with PLA staple cut to 6–12 mm in a spiked-roll forming head and deposited onto a tissue carrier. Thermal bonding occurs on an embossed calender with roll surface temperatures in the 120–145°C range and nip pressures of 40–80 N/mm; because 6060D is amorphous and exhibits no crystalline melting endotherm, the calender temperature must be mapped against machine-direction tensile strength determined by ISO 9073-3:2023. The process window is narrower than for a crystalline PLA because the fibre softens progressively above its glass transition near 55–60°C, and an overbonded web loses caliper before tensile failure is observed. Thickness is measured by ISO 9073-2:2023, and hygiene converters additionally control bioburden under ISO 11737-1:2018. The terminal product is a pre-bonded airlaid absorbent core in which superabsorbent polymer is metered between bonded and unbonded layers without disturbing the thermal seal.
Substitution with 6060D amorphous PLA staple in through-air bonded acquisition layers removes the defined melting plateau that makes polyethylene/polypropylene bicomponent fibres tolerant of overheat. A perforated drum through-air oven running air temperatures of 115–135°C, dwell times of 3–8 s, and air velocities of 0.5–1.5 m/s can bond the PLA web, but the setpoint tolerance on the drum face is typically reduced to about ±3°C because the amorphous fibre continues to soften and flatten as temperature moves above the glass transition. Bond strength develops through chain interdiffusion at fibre crossover points, while excess heat simultaneously collapses void volume and increases film-like bridging. The process conflict is that tensile strength measured by ISO 9073-3:2023 and liquid handling measured by ISO 9073-13:2006 move in opposite directions at the upper end of the bonding window. An acquisition layer of 40–60 gsm with a high strike-through delay is unacceptable for hygiene use even if dry tensile strength is adequate. Because the 6060D fibre surface softens near 60°C, start-up trials must map oven temperature against tensile, caliper, and repeated liquid strike-through time as separate responses rather than assuming that higher bond strength improves the product.
For a soil-contact weed suppression fabric made from 100% 6060D carded web, the specification is governed by soil burial disintegration and tensile stability during the crop cycle, not by absorbency or loft. A 200–300 gsm web is cross-lapped to control the machine-direction/cross-direction tensile ratio and needlepunched at a needle density of 80–120 penetrations/cm²; needle barb depth and penetration depth are set to avoid cutting the staple, which would create short fibre fragments that degrade faster than the continuous fibre network. Tensile strength is measured by ISO 9073-3:2023, tear strength by ISO 9073-4:2023, and the cross-lap angle is adjusted so that the MD/CD tensile ratio is kept between 1.2:1 and 2.0:1 to prevent diagonal tearing during field installation. Aerobic biodegradation of the polymer matrix is tested under ISO 14855-1:2012 at 58°C and 50% relative humidity, which gives a mineralization percentage under industrial compost conditions; ambient soil-contact degradation is slower and must be assessed under ASTM D5988-18. The terminal product is a biodegradable weed barrier for annual horticultural beds that can be left in the field only where soil temperature and moisture meet the specified compost or soil degradation conditions.
In heat-sealable filter paper for tea bags and single-serve coffee pods, 6060D staple cut to 6–12 mm is blended with bleached softwood kraft pulp at 5–15 wt% fibre mass. The wetlaid furnish is dispersed at headbox consistency of 0.02–0.05% and formed on an inclined wire; because amorphous PLA staple is hydrophobic, a nonionic surfactant is added at 0.1–0.5 wt% on fibre to reduce flocculation and prevent rope formation. Sheet drying is run through through-air dryers or contact dryers at 100–120°C, which softens the PLA surface sufficiently for seal activation without brittling the cellulosic matrix. Heat-seal strength is measured by ASTM F88/F88M-21 on 15 mm sealed strips, and dry tensile strength is measured by ISO 1924-2:2008. Food contact migration is tested under EC No 10/2011 using simulant D1 water at 100°C for 2 h, with overall migration below 10 mg/dm² required for the specific article. Because the 6060D glass transition is near 55–60°C, boiling water exposure can soften unbonded amorphous PLA domains; the paper web must constrain the PLA through mechanical entanglement and hydrogen bonding with cellulose to prevent distortion. The terminal product is a heat-sealable filter paper with a seal temperature substantially lower than that required by polypropylene spunbond and without a solvent-based seal coating.
Flushable wipes made with 6060D staple use a furnish of bleached hardwood and softwood pulp at 70–85 wt% and PLA fibre at 15–30 wt%, cut to 4–8 mm to survive hydroentangling without wrapping around forming wire rolls. Stock preparation requires a nonionic or amphoteric dispersant at 0.1–0.5 wt% on dry fibre and a neutral pH range of 6.5–7.5 because prolonged alkaline pH promotes PLA hydrolysis at the fibre surface. Headbox consistency of 0.01–0.05% and high stock dilution prevent PLA fibre aggregation, which appears as translucent fused clumps after through-air drying. Hydroentangling at 60–120 bar hydraulic pressure entrains the PLA staple into the cellulosic matrix and reduces linting; subsequent thermal bonding at 110–130°C on a through-air drum activates the amorphous PLA surface and closes the sheet, but overdrying embrittles the cellulosic fraction and reduces dispersibility in wastewater. The finished wipe is tested under the INDA/EDANA GD4 flushability assessment protocol, including municipal pump and settling tests. The PLA fraction is considered compostable under industrial composting conditions such as ISO 16929:2021, not under short residential sewage residence times. The terminal product is a dispersible wet wipe with sufficient wet strength during use and a designed failure point at sewer turbulence.
| Application scenario | Test method designation | Measured control parameter |
|---|---|---|
| Airlaid absorbent core | ISO 9073-3:2023, ISO 9073-2:2023 | Dry tensile strength, caliper after thermal bonding |
| Through-air acquisition layer | ISO 9073-13:2006, ISO 9073-3:2023 | Repeated strike-through time, dry tensile strength |
| Needlepunched weed barrier | ISO 14855-1:2012, ASTM D5988-18 | Mineralization percentage, soil burial strength retention |
| Heat-sealable filter paper | ASTM F88/F88M-21, EC No 10/2011 | Seal strength, overall migration |
| Flushable wipes | INDA/EDANA GD4, ISO 16929:2021 | Flushability, pilot compost disintegration |
| Acoustic absorber panel | ISO 9053-1:2018, ISO 354:2003 | Airflow resistivity, sound absorption coefficient |
| Fibrefill batting | ISO 9073-2:2023 | Thickness recovery after conditioned compression |
Vertical-lapped acoustic absorber panels incorporating 6060D staple are processed by carding, cross-lapping or vertical lapping into a batt of 20–40 kg/m³ target density, then passing through a hot-air oven where the amorphous PLA fibre bonds at crossover points. Airflow resistivity is measured by ISO 9053-1:2018, and the sound absorption coefficient is measured by ISO 354:2003 in a reverberation room; panel thickness is set between 25 mm and 50 mm to tune low-frequency absorption while retaining panel rigidity. Because 6060D has a glass transition near 55–60°C, continuous service temperature for an unbonded amorphous PLA panel is limited to below approximately 50°C, which excludes direct contact with lighting ballasts or building service pipes. Flame-spread and smoke development are not intrinsic properties of PLA and must be addressed by additive formulation or panel construction; untreated PLA staple will not meet EN 13501-1 Class B without flame-retardant treatment, and any additive must be evaluated for migration and for interference with the thermal bonding window. The terminal product is an acoustic absorber for interior wall and ceiling installations where temperature and fire loads are controlled by specification.
Fibrefill batting for mattress quilt panels and pillow inserts uses crimped staple opened in a garnett and air-laid into a continuous batt of 60–120 gsm per layer, with 6060D acting as a binder fibre at 20–30 wt% in blends with crimped semi-crystalline PLA or recycled polyester. The batt is passed through a forced-air oven at 110–135°C for 2–5 min to soften the amorphous PLA surface and bond crossover points; excessive residence time at temperature collapses loft because the amorphous phase continues to deform under the batt’s own weight and airflow pressure. Thickness recovery is evaluated under ISO 9073-2:2023 after conditioned compression, and the line must distinguish between thermal collapse and normal compression set during storage. Wet heat above 60°C accelerates PLA hydrolysis and loss of crimp, so the fibrefill is not specified for repeated hot-water washing at high temperature. The terminal product is a low-density fibrefill batting for mattress quilt panels where service temperature remains below approximately 45°C and compression recovery is controlled by batt construction and bond-point density.
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NatureWorks Ingeo™ Biopolymer 6060D Amorphous Fiber-Grade Staple Fiber PLA is a fiber-grade polylactide tailored for staple-fiber melt spinning and downstream thermally bonded nonwoven, wadding, and fiberfill conversion. The grade is specified by the supplier with a nominal density of 1.24 g/cm³ under ASTM D792; melt flow index is tested under 210°C/2.16 kg using ASTM D1238 and is commonly released within the fiber-spinning band of 15–30 g/10 min, although exact values must be verified against the lot certificate of analysis. Differential scanning calorimetry under ASTM D3418 indicates a glass transition near 55–60°C and no sharp crystalline melting endotherm above 160°C, placing 6060D in the amorphous fiber-grade class. The grade is intended for conversion where thermal bonding, lower bonding temperature, and controlled stiffness are primary design variables rather than high-tenacity crystalline fiber performance.
Moisture control is the primary boundary condition during conversion. Resin should be dried in a desiccant dryer at 80°C for 4 h to a residual moisture below 250 ppm; on production lines, a desiccant-bed dew point of ≤-40°C and hopper-mounted dry-air sweep are frequently required because ambient relative humidity above 60% can raise surface moisture uptake beyond the target within 30 min. Hydrolytic chain scission is the limiting degradation mechanism: above 230°C melt temperature with moisture above 250 ppm, random ester cleavage can be detected as a melt flow index rise of 5–10 g/10 min within 10 min residence. Barrel set points on single-screw extruders with 24:1–30:1 L/D are typically 180–220°C; spin-head temperature is limited to 225°C, and total residence time above 230°C is held below 15 min.
Capillary rheometry with ISO 11443 at 210°C shows shear-thinning behavior typical of PLA; the apparent viscosity at 1000 s⁻¹ remains in a range that imposes moderate spin-pack pressures. Spinneret melt distribution channels should avoid dead spaces greater than 3 mm, because stagnation increases residence time and gel formation. On a 75 mm single-screw extruder with 30:1 L/D, screw speeds above 80 rpm at pack pressures above 120 bar have been associated with melt-temperature overshoot; field reports describe reducing barrel zone set points by 5–10°C to compensate. This threshold is operationally significant because amorphous PLA has no crystalline melting endotherm to buffer overheating.
| Property | Test method | Typical value | Processing relevance |
|---|---|---|---|
| Density | ASTM D792 | 1.24 g/cm³ | Throughput calibration and blend ratio calculation |
| Melt flow index at 210°C/2.16 kg | ASTM D1238 | 15–30 g/10 min | Spin-pack pressure, draw tension, and melt strength |
| Glass transition | ASTM D3418 | 55–60°C | Thermal bonding and heat-set threshold |
| Residual moisture | ASTM D7191 / ISO 15512 | <250 ppm | Hydrolytic degradation prevention |
| Crystalline melting endotherm | ASTM D3418 | Absent above 160°C | Distinguishes amorphous bonding response |
Pre-extrusion blending of 6060D with semi-crystalline PLA regrind is not recommended above 2.5 wt%. At higher levels, differences in crystalline melting and recrystallization can generate hard particulate in the spin pack and accelerate filter pressure rise. Continuous staple lines typically use filter media of 20–40 µm; a pressure-rise rate above 0.5 bar/h at constant throughput generally indicates contamination, regrind carryover, or moisture-induced gel formation. Amine-based antistatic or flame-retardant masterbatches should not be introduced without prior thermal stability screening under ISO 11358 and melt-flow stability verification under ISO 1133-1:2022. Residual alkalinity carried by such additives can promote lactide reformation and reduce fiber tensile strength, even when the base resin itself is dry.
The defining difference is the thermal response measured by DSC. Semi-crystalline fiber-grade PLA typically shows a melting endotherm in the 150–165°C region, while 6060D shows only the glass transition near 55–60°C and a broad softening range. This shifts calender bonding set points for carded webs downward by approximately 20–40°C. Bending stiffness of the bonded fabric, when measured under ISO 9073-7, is therefore controlled more by bond shape and calender pressure than by polymer melting enthalpy. The amorphous grade is commonly drawn to 2.5:1–3.5:1; higher draw ratios can induce strain-induced crystallization and reduce the available low-temperature bonding window. Published data for this specific configuration is limited, so mill trials should compare bonding temperature, line speed, and fabric stiffness using a factorial design.
| Characteristic | Ingeo 6060D amorphous fiber-grade | Semi-crystalline fiber-grade PLA reference |
|---|---|---|
| DSC melting endotherm | Absent above 160°C | 150–165°C |
| Thermal bonding calender window | 90–120°C | 130–150°C |
| Typical staple draw ratio | 2.5:1–3.5:1 | 3.0:1–5.0:1 |
| Fiber tenacity at standard draw | 25–35 cN/tex | 35–50 cN/tex |
| Continuous service above 60°C | Limited without application-specific validation | More dimensionally stable after heat setting |
On a two-stage staple fiber line, dried 6060D is melted in a single-screw extruder and pumped through a spin pack with capillary diameters of 0.3–0.8 mm. Quench air at 10–20°C is used to stabilize filaments; finish is applied before crimping at 0.15–0.30 wt% on fiber, and the crimped tow is cut to staple lengths of 38–51 mm or 60–90 mm depending on carding configuration. Melt-flow variation across the 15–30 g/10 min band can change draw tension and crimp take-up; when the melt flow index approaches 30 g/10 min, draw-stand speed may require reduction to prevent filament breaks and crimp instability. Fiber tensile properties are measured by ASTM D3822 or ISO 5079; at the draw ratios common for this grade, single-fiber tenacity is typically reported in the 25–35 cN/tex range and elongation at break between 30% and 50%, though exact values depend on finish, draw ratio, and quench uniformity.
Fabric-level characterization follows the nonwoven test series: mass per unit area by ISO 9073-1, thickness by ISO 9073-2, tensile strength by ISO 9073-3, tear resistance by ISO 9073-4, and stiffness by ISO 9073-7. These methods are not resin certifications, but they are required to translate fiber properties into application acceptance criteria. When 6060D is used in hygiene or medical nonwovens, bond strength and linting behavior should be evaluated under IST 90.3 or comparable INDA/EDANA test methods; published data for this specific configuration is limited.
Because the resin is amorphous, carded webs and fiberfill made from 6060D cannot be heat-set to the dimensional stability of semi-crystalline PLA. Shrinkage testing under ISO 1897 or ASTM D2259 should be performed on finished articles before specifying continuous use above 60°C. Post-bonding cooling must be controlled before winding to prevent blocking and distortion. The grade is not intended for high-tenacity technical textiles in which semi-crystalline PLA drawn above 4:1 is used to reach fiber tenacities above 30 cN/tex. Regulatory compliance for food-contact, medical, or composting end uses is not automatic; finished-article migration testing under EU 10/2011, 21 CFR 175.300, or ISO 10993 is required where applicable. Lot-specific REACH and RoHS statements should be requested from the supplier if certification documentation is required by downstream converters.
Biobased carbon content can be quantified by ASTM D6866 or ISO 16620-2; PLA derived from lactic acid fermentation typically exceeds 95% renewable carbon, though this is a feedstock declaration rather than a finished-article property. The amorphous grade is not a direct replacement for semi-crystalline fiber grades on high-speed spunbond lines, because the lower crystallization rate and bonding window change draw stability. Processors switching from a semi-crystalline staple grade should not assume existing calender settings, quench profiles, or draw ratios transfer without trial.