| HS Code | 111266 |
| Density Conditioned | 1.04 g/cm³ |
| Water Absorption 24h | 0.9 % |
| Tensile Modulus Conditioned | 1200 MPa |
| Yield Stress Conditioned | 35 MPa |
| Yield Strain Conditioned | 20 % |
| Nominal Strain At Break Conditioned | >50 % |
| Charpy Impact Strength Notched 23 C Conditioned | 35 kJ/m² |
| Charpy Impact Strength Notched 30 C Conditioned | 12 kJ/m² |
| Melting Temperature Dsc | 178 °C |
| Heat Deflection Temperature Hdt 1 8 Mpa | 50 °C |
| Vicat Softening Temperature 50 N | 145 °C |
As an accredited Evonik VESTAMID® X7293 BK 9.7507 Nylon 12, Conditioned factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.
| Packing | Evonik VESTAMID® X7293 BK 9.7507 Nylon 12, Conditioned is supplied in 25 kg sealed, moisture-protective polyethylene-lined bags. |
| Container Loading (20′ FCL) | 20′ FCL: palletized nylon 12 granules, secured with dunnage, moisture-protected, ventilated, loaded per weight limits safely. |
| Shipping | Evonik VESTAMID® X7293 BK 9.7507 Nylon 12 (Conditioned) ships as non-hazardous thermoplastic pellets. Pack in sealed, moisture-resistant containers to preserve conditioned state. Store in cool, dry area away from direct sunlight and heat. Standard truck or rail transport is suitable, with protection from rain and humidity during loading and transit. |
| Storage | Store Evonik VESTAMID® X7293 BK 9.7507 Nylon 12 in its original, sealed container to preserve its conditioned state. Keep in a cool, dry area away from direct sunlight, heat sources, and excessive humidity. Avoid moisture absorption, which can alter properties. Reseal packaging tightly after each use. Follow manufacturer guidelines. |
| Shelf Life | Shelf life is typically two years from shipment date when stored in original, unopened packaging under dry, cool conditions. |
On production lines extruding 10 mm outside-diameter truck air brake tubing from VESTAMID X7293 BK 9.7507, single-screw machines with 24:1 to 30:1 L/D barrels and three-zone screws feed a crosshead die mounted with a static mixer. The conditioned state is a manufacturer-adjusted moisture level; it does not replace closed-loop drying once the package has been opened above 60% RH for more than 3 hours. Surface moisture uptake changes melt viscosity and can generate longitudinal weld lines at the die spider. A desiccant dryer with -40°C dew point and 80°C air temperature for 4 to 6 hours is the corrective step to return pellet moisture below 0.1%. Typical start-point barrel temperatures range from 195°C to 240°C from feed to metering zones, with head and die temperatures held at 230°C to 235°C. A 10 mm OD, 1.0 mm wall tube is commonly produced at 2.0 to 2.8 m/min haul-off speed with melt pressure between 20 and 35 MPa. Wall-thickness variation is maintained at ±0.05 mm under DIN 73378 and ISO 7628-1 tolerance classes. The black pigment package in the 9.7507 colour designation absorbs UV and slows photo-oxidation; xenon-arc testing according to ISO 4892-2 is used to detect surface crazing. Cold impact is checked at -40°C for 30 minutes followed by mandrel bending; no visible cracking is the acceptance condition. In service, the compressor discharge segment carries compressed air, mineral oil mist and water aerosol at peak temperatures above 85°C. The dominant interface failure is creep rupture at the ferrule caused by plasticizer migration into the oil layer, not tensile burst. Leak-tight function requires ferrule compression settings matched to the conditioned PA12 Shore D range of 55 to 62 and tube OD shrinkage of no more than 0.1 mm after 100°C dry-air ageing for 72 h.
| Parameter | Range or setting | Measurement point |
|---|---|---|
| Screw L/D | 24:1 to 30:1 | Extruder frame |
| Screw compression ratio | 2.5:1 to 3.0:1 | Feed-to-metering channel depth |
| Feed zone temperature | 195°C to 205°C | Barrel zone 1 |
| Metering zone temperature | 235°C to 240°C | Barrel zone 3 |
| Head/die temperature | 230°C to 235°C | Crosshead die body |
| Melt moisture target | < 0.1% | Karl Fischer titration of pellet sample |
| Desiccant dryer dew point | -40°C | Drying hopper outlet |
| Cooling water temperature | 25°C to 45°C | Vacuum sizer tank, first stage |
| Line speed for 10 mm OD, 1.0 mm wall | 2.0 to 2.8 m/min | Haul-off encoder |
The limiting variable is ovality at the inner bend, not the flexural modulus of the conditioned PA12 alone. For a 10 mm OD tube bent to a static radius of 60 mm, the calculated outer-wall bending strain is approximately 8.3%, assuming neutral-axis displacement through the centroid. At 45 mm radius, the calculated strain rises to 11.1%, placing the inner-wall compressive side under plastic strain and increasing ovalization to the point where a push-in fitting can disengage. At -40°C, the conditioned matrix retains tensile strain at break above 50% when tested according to ISO 527-2/1B, but cold-induced stiffening raises the force required to re-round the tube inside a spiral-cut HDPE harness. The spiral wrap acts as a series of discrete bending constraints. Tubing that passes a free-air mandrel bend can still whiten at the spiral gaps because localized bending strain concentrates between adjacent HDPE coils. On assembly lines, spiral-wrap tension is therefore limited to 1.0 to 2.0 N for a 10 mm tube to avoid pre-loading the outer wall. Air brake specification ISO 7628-1 and SAE J844 require cold flexibility after conditioning; the specific acceptance threshold for spiral harness installations is usually set by the fitting manufacturer rather than the tubing standard. A production audit of failed harnesses generally records that the tube was bent below 8 × OD at ambient temperature, producing immediate inner-wall compression creases. These creases do not reduce initial burst pressure; they reduce fatigue life under pressure impulse because the crease root acts as a stress concentration. The conditioned moisture level matters here because an over-dried tube extruded below 0.05% moisture can exhibit higher melt viscosity and greater die swell, increasing initial ovality and leaving less margin for harness bending. Conversely, residual moisture above 0.15% creates surface micro-voids at the inner wall after cooling that open into visible micro-cracks when the tube is installed on a tight-radius jig.
Inside commercial vehicle chassis wiring harnesses, VESTAMID X7293 BK 9.7507 is extruded as a smooth or corrugated jacket over copper or aluminium conductor bundles where ISO 6722-1 abrasion, chemical and low-temperature tests apply. For a single-layer jacket with wall thickness 0.25 to 0.50 mm, the black PA12 compound is selected because it combines low-temperature flex without cracking and resistance to diesel mist and road salt. Jacketing line speeds typically run between 80 and 150 m/min for thin-wall smooth cable sheaths; vacuum sizing is adjusted so final diameter tolerance remains within ±0.05 mm. The conditioned resin is dried below 0.1% moisture before jacketing because surface moisture in the carbon-black PA12 melt can generate pinholes at wall thicknesses below 0.2 mm. Abrasion and chemical tests follow ISO 6722-1 methods; exact abrasion-cycle limits for this specific compound are controlled by the OEM specification, and published data for this configuration is limited. Salt-spray exposure according to ISO 9227 for 480 h is applied to verify resistance to chloride road spray after jacket extrusion. Ultraviolet exposure is evaluated by ISO 4892-2 xenon-arc testing for 1000 h; the black carbon package should show no chalking and a colour shift not greater than 5 CIELAB units on the outer surface. The jacket is not intended for continuous immersion in hot glycol-based brake fluid above 70°C because plasticizer extraction by polyglycol ethers can produce swelling greater than 5% mass change and loss of jacket dimensional stability. Fill ratio inside corrugated conduit is limited to 70% maximum, with corrugation pitch of 4 to 6 mm, to control internal abrasion against conductor insulation during chassis flexing.
The thermal boundary of VESTAMID X7293 BK 9.7507 in an air brake discharge line is not set by dry heat deflection alone, but by the combined action of condensed mineral oil, water aerosol and brass fitting ions. At compressor outlet temperatures of 120°C to 140°C, the first 100 to 150 mm of nylon tube downstream can see surface temperatures above 100°C, which accelerates plasticizer migration into the condensed oil film. The inner-wall oil layer absorbs low-molecular-weight plasticizer fractions; when the tube cools and the oil drains back into the reservoir, the PA12 matrix shrinks in the clamping zone and ferrule retention force drops. This loss of clamping force is quantifiable by pull-off force testing after 1000 h oil ageing at 100°C; a drop of more than 25% from the initial pull-off value is the usual replacement threshold. Hydrolysis is a second parallel mechanism. Air discharged from a compressor reaches the tube saturated with water vapour; at local temperatures above 85°C, steam condensation inside the tube accelerates cleavage of the PA12 amide linkages. Gel permeation chromatography of the inner-wall extract after cyclic damp-air exposure is used to monitor molecular-weight shift; published data for this specific formulation is limited. The first 100 to 150 mm from the compressor port should therefore be routed through a metallic transition assembly or shielded with an air gap to keep the nylon tube below 110°C. Direct clamping to a hot compressor manifold is not permitted because local wall temperature above 110°C causes a sharp decline in oxidative induction time. The grade is not intended for continuous contact with glycol-based brake fluids above 70°C; polyglycol ethers can extract plasticizer and produce mass change greater than 5%. Where an OEM requires SAE J844 performance, the heat-ageing sequence of 100°C for 72 h must be followed by a burst test at 23°C and a cold impact test at -40°C, with no inner-wall cracking allowed.
| Application | Reference standard | Critical test condition | Pass criterion |
|---|---|---|---|
| Air brake tubing | SAE J844, ISO 7628-1 | 100°C ageing 72 h, then -40°C impact | No crack at mandrel bend |
| Heat and oil contact | ISO 1817 | Mineral oil 72 h at 23°C | Volume change ±4% maximum |
| UV weathering | ISO 4892-2 | Xenon arc 1000 h | No chalking, ΔE ≤ 5 |
| Chassis cable jacket | ISO 6722-1 | Low temperature -40°C | No insulation damage after flex |
In automated assembly and welding cells, a 10 mm OD × 1.0 mm wall PA12 tube operating at 0.6 MPa compressed-air pressure has a calculated hoop stress of approximately 2.6 MPa, while the conditioned grade retains a tensile yield stress above 25 MPa at room temperature. The pressure margin is not the limiting factor. The limiting factor is torsional shear accumulated at the robot wrist, where a tube can be twisted ±180° several times per cycle. Each reversal displaces the neutral axis and creates diagonal shear bands in the outer wall. These bands appear as white stress-whitening marks under optical microscopy before through-wall cracking occurs. A failed service loop in an automotive body shop can lose pull-off retention after combined bending and torsion; the exact loss is determined by fitting-level validation, not by the material alone. When 500,000 cycles of combined flex and torsion are specified, the pass criterion is typically no leakage at 2.0 MPa with the fitting in place. The PA12 matrix is selected for this duty because the ether-free amide chain provides low friction against polyurethane or HDPE spiral wrap and because the conditioned material retains useful flexibility down to -40°C, enabling cold-start robot moves without jacket split. Tube design for robot dress packs follows ISO 4414 for pneumatic system safety and ISO 14743 for pneumatic tube dimensions and installation. The acceptable minimum dynamic bend radius for PA12 is generally 12 × OD; when the robot cell requires a 10 mm tube to flex inside a 70 mm radius wire carrier, a PA12 grade with Shore D hardness below 60 is necessary to prevent brittle cracking at the corrugation hinge points. Dry regrind should not be blended above 20% without re-qualification, because regrind lowers spiral-flow length and increases weld-line porosity at the fitting end.
Where stone impact and high-pressure wash detergents define the operating envelope in construction and agricultural machinery, VESTAMID X7293 BK 9.7507 is routed as air seat suspension hose, transmission shift-assist tubing and cab tilt system lines. These applications subject the tube to mud packing, stone impact and alkaline wash detergents. Abrasion resistance is tested with a 5 N scraper load against an aluminium oxide surface; the pass requirement is a wear scar depth less than 0.2 mm for a 1.0 mm wall. Diesel fuel and hydraulic oil splash resistance is confirmed by immersion according to ISO 1817 in reference fuel and mineral oil for 72 h at 23°C, with a maximum volume change of ±4% and no visible surface tack. Because the equipment operates at -35°C to +85°C ambient, the tubing must survive thermal shock from engine-bay heat to cold air without cracking at the fitting insert, which is assessed by 10 cycles of -40°C to 100°C with a dwell time of 2 h at each extreme. The black formulation protects against UV during roof storage; after 1000 h of ISO 4892-2 exposure, the surface should show no chalking and retain at least 80% of original tensile elongation at break. Installation on stone-impact zones requires spiral wrap or split loom; direct exposed runs on the underside of a wheel loader are an off-spec condition unless the OEM validates impact resistance after defined-impact testing at -40°C. The most frequent field failure is not chemical degradation but cut-through from chafing against zip ties and steel hose clamps. The tube is clamped only with smooth-edge plastic P-clips and a maximum strap width of 12 mm; metal worm-gear clamps are not used because they create local stress concentration that reduces burst pressure by 20 to 30% when tightened beyond 2 N·m.
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Evonik VESTAMID® X7293 BK 9.7507 Nylon 12, Conditioned identifies a black-pigmented polyamide 12 compound whose data-sheet property set is reported after controlled moisture uptake. The product identifier consists of the VESTAMID registered family, the X7293 compound modifier, the BK black colour designation, and the internal formulation code 9.7507. In this context, “Nylon 12, Conditioned” is a test-state descriptor rather than a guarantee that the granulate leaves the plant with a fixed water content. Conditioned values are generally generated after exposure to 23 °C and 50 % relative humidity according to ISO 291, or after accelerated conditioning for polyamides under DIN EN ISO 1110. The formal specification block under ISO 1874-1 would require the supplier-reported viscosity class, tensile modulus class, and impact class for the specific black formulation; the commercial code X7293 BK 9.7507 is not itself an ISO designation. The black grade is positioned for extrusion and injection moulding where carbon black provides weathering resistance and the lower moisture uptake of PA12 compared with PA6 or PA66 is required.
Polyamide 12 absorbs water through hydrogen bonding at amide groups, but the long aliphatic C12 backbone reduces the concentration of amide groups relative to short-chain polyamides. At equilibrium in 50 % relative humidity, unmodified PA12 commonly takes up approximately 0.6 % to 0.8 % water by mass; saturated water uptake is measured separately under ISO 62. Moisture uptake is diffusion-limited and thickness-dependent. A 4 mm tensile bar develops a through-thickness moisture profile over a longer period than a 0.2 mm film, and this gradient can temporarily produce a stiff skin with a tougher core. In the conditioned state, the absorbed water plasticizes amorphous regions, lowers the glass transition, reduces tensile modulus, and increases elongation at break. For polyamide 12, the conditioned tensile modulus is frequently between 50 % and 70 % of the dry-as-moulded value, but the exact ratio for VESTAMID X7293 BK 9.7507 is supplier-specific and influenced by the modifier package. Carbon black does not eliminate this response; it may slightly reduce the moisture diffusion rate and increase density, but the equilibrium moisture content of the polyamide phase remains governed by humidity. Conditioned Charpy impact values under ISO 179-1/1eA are usually higher than dry values because matrix plasticization reduces notch sensitivity. For press-fit joints and connector retention, moisture-induced swelling can alter dimensions after installation if a dry part is exposed to humid air. Dry-as-moulded data should therefore be used for demoulding and short-term load cases, while conditioned data are more representative for humid service and liquid-contact environments.
Pneumatic tubing and fuel-vapour lines are among the more demanding applications for this black PA12 class. Tube extrusion operations use vacuum sizing to control diameter and wall thickness, and carbon black dispersion becomes a quality parameter because an agglomerate can create a pinhole or a stress concentration under burst testing. Conditioned mechanical values are used to predict installation force, clamp retention, and flexibility after the tube has equilibrated with ambient moisture. In truck air-brake tubing, the material must maintain circularity during sizing, resist zinc chloride from road de-icing, and retain low-temperature flexibility. Ultraviolet protection from the black colorant is validated by accelerated weathering under ISO 4892-2 or OEM-specific environmental cycles rather than by colour content alone. The exact certification status of VESTAMID X7293 BK 9.7507 under specifications such as SAE J844 or DIN 73378 should be confirmed against supplier release documentation; published data for this specific commercial configuration is limited outside the controlled datasheet.
Conditioned mechanical data are generated with water present, but melt processing requires the absence of water. This creates an operational conflict: a moulding or extrusion line that treats the conditioned label as a processing instruction risks hydrolysis, surface splay, pressure instability, porosity, and viscosity loss. The same moisture that improves toughness in the finished component is harmful at melt temperature. Before processing, the granulate should be dried in a desiccant dryer with a dew point below −30 °C. Typical PA12 drying conditions are 80 °C for 4 h to 6 h, with a residual moisture target below 0.10 % to 0.15 %. Excessive drying temperature can oxidize the black surface and cause yellowing, so the supplier limit should not be exceeded.
Single-screw extrusion of black PA12 is more demanding than extrusion of natural grades because carbon black increases melt viscosity and can form agglomerates. A polyamide screw with an L/D ratio between 25:1 and 30:1, a compression ratio of 2.5:1 to 3.0:1, and a mixing section is preferred for dispersion. Melt temperature is typically held between 210 °C and 240 °C, although the X7293 additive package may narrow the acceptable window because plasticizer or impact-modifier components can limit thermal stability. Melt pressure before the screen pack should be monitored; a steady rise toward 200 bar can indicate filter blockage from carbon black agglomerates or degraded gel particles. In injection moulding, moisture also alters melt viscosity and affects screw recovery time, cushion position, and switchover point. Tool temperatures from 60 °C to 90 °C are common for PA12 to achieve sufficient crystallinity and dimensional stability. Regrind use should follow the supplier technical bulletin; excessive regrind lowers viscosity and increases gel formation because of the additional heat history.
Cable sheathing and connector overmoulding represent a further use area. The black grade supplies weathering resistance for outdoor cable constructions, but outdoor performance is verified by exposure testing rather than by carbon black content alone. In electrical connectors, conditioned PA12 absorbs water that increases ionic mobility and lowers volume resistivity relative to the dry state. The dissipation factor also rises with moisture content, so dry dielectric data are not conservative for humid service. If the component is used at elevated voltage, the specific dielectric performance must be validated; PA12 is not automatically suitable for high-voltage insulation. Thin-wall overmoulding requires sufficient melt flow to fill long paths without premature freeze-off, and oil-heated tooling supports crystallization and surface appearance. The conditioned label of the feedstock is not relevant during moulding because the granulate must be dried before melting.
Compared with a natural unmodified VESTAMID PA12 grade, the X7293 BK 9.7507 formulation contains a black pigment and a modifier package that changes flow behaviour and mechanical response. The black pigment raises melt viscosity and density but improves weathering resistance. The X-series identifier indicates a modified product, though the exact chemistry is not defined by a public ISO code. Against PA11, PA12 offers comparable low-temperature flexibility and somewhat lower saturated water uptake; both have long aliphatic backbones and are used in automotive tubing. Against PA6 and PA66, PA12 shows markedly lower conditioned moisture uptake and less property loss between dry and humid states, but its dry tensile modulus and heat deflection temperature are lower. The difference is greatest in the conditioned state because PA6 and PA66 may absorb several percent water at saturation, which reduces stiffness and shifts dimensions. Against polyether block amide elastomers, the X7293 compound is a semi-flexible modified polyamide rather than an elastomer: it has higher modulus, higher crystalline melting point, and lower ultimate elongation, with less elastic recovery and less low-temperature softness.
| Test property | Standard method | Conditioning relevance |
|---|---|---|
| Density | ISO 1183-1 | Black formulation typically above natural PA12 density |
| Water absorption at equilibrium | ISO 62 / DIN EN ISO 1110 | Defines conditioned test specimen preparation |
| Tensile modulus, stress at break, elongation | ISO 527-1/2 | Values differ between dry and conditioned states |
| Charpy notched impact | ISO 179-1/1eA | Conditioned specimens often show higher absorbed energy |
| Melting peak | ISO 11357-1/3 | PA12 backbone melting is independent of conditioning |
| Melt volume-flow rate | ISO 1133-1 | Requires dry feedstock; moisture alters flow |
One operational conflict is that conditioned mechanical data describe a service condition, while the same moisture content is detrimental during melt processing. If a datasheet lists only conditioned values, there is a documentation risk that the moulder or extruder processes the granulate without drying because the label says “Conditioned.” The result can be hydrolysis, pressure variation, black speck formation, and reduced molecular weight. Conversely, designing a component from dry values and then exposing it to high humidity can produce unexpected dimensional growth and stiffness loss. The production line should maintain separate specifications: dry feedstock for processing and conditioned test data for service performance. Moisture equilibration in a finished part is not instantaneous; thick-walled components may remain dry in the core for months, leading to dimensional drift and residual stress. Post-mould conditioning may therefore be required before final dimensional inspection when the component is intended for humid service.