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Evonik VESTAMID® LX9008 PA 12

    • Product Name: Evonik VESTAMID® LX9008 PA 12
    • Factroy Site: Yudu County, Ganzhou, Jiangxi, China
    • Price Inquiry: admin@ascent-chem.com
    • Manufacturer: Ascent Petrochem Holdings Co., Limited
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    Specifications
    HS Code 791682
    Material Evonik VESTAMID LX9008 PA12
    Product Form Fine powder for laser sintering
    Bulk Density 0.45 g/cm³
    Sintered Density 0.96 g/cm³
    Melting Temperature 178 °C
    Crystallization Temperature 141 °C
    Tensile Modulus 1600 MPa
    Tensile Strength 48 MPa
    Elongation At Break 25 %
    Charpy Impact Strength Unnotched 30 kJ/m²
    Shore D Hardness 75
    Particle Size D50 55 µm

    As an accredited Evonik VESTAMID® LX9008 PA 12 factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing Evonik VESTAMID® LX9008 PA 12 is supplied as dry granules, packaged in sealed 25 kg bags.
    Container Loading (20′ FCL) 20′ FCL container shipment of Evonik VESTAMID® LX9008 PA12, securely packed and braced for safe transport.
    Shipping VESTAMID® LX9008 PA 12 is supplied as moisture-sensitive pellets in sealed bags. Ship in clean, dry containers or covered trucks to prevent humidity exposure. Avoid excessive heat or pressure during transit. Store cool and dry. Standard non-hazardous handling applies, with proper labeling and documentation.
    Storage Store VESTAMID® LX9008 PA 12 in its original, unopened packaging in a cool, dry place away from direct sunlight and heat sources. Keep containers tightly sealed to prevent moisture absorption, which can degrade the polymer. Under these conditions, typical shelf life is at least one year.
    Shelf Life Store in cool, dry conditions in original sealed packaging. Typical shelf life is 12 months from delivery.
    Application of Evonik VESTAMID® LX9008 PA 12

    What Drives Thermoplastic Selection in Air Brake Lines for Class 7–8 Vehicles?

    In heavy-duty commercial vehicle pneumatic braking circuits, the tube wall is subjected to repeated pressure pulses between 0 MPa and 1.0 MPa, ambient temperatures from −40°C to +100°C at the compressor discharge, and continuous vibration across frame crossmembers. VESTAMID® LX9008 is processed as the base polymer in monolayer tube extrusion because the plasticized PA12 backbone reduces low-temperature brittle fracture risk after cold-weather parking. Production runs for air brake tube are not based on neat resin alone: 95.0–98.0 wt% predried base resin is dry-blended with 2.0–5.0 wt% colorant/heat-stabilizer masterbatch; the exact let-down ratio is adjusted until the extruded wall meets the opacity and thermal-oxidative performance required by the tube print legend and vehicle OEM line specification. Pellets must be dried to <0.10 wt% moisture in a desiccant dryer at 80°C for 4–6 h before extrusion, because residual moisture above this limit produces hydrolysis at processing temperature and pinholes that fail the SAE J844 pressure-decay requirement. Extrusion is performed on a single-screw extruder with L/D 30:1, a barrier screw with a dispersal mixing section, and a screen pack of 60/80/100 mesh. Barrel set points from feed to die typically progress 210°C / 220°C / 230°C / 235°C / 240°C, with melt temperature held between 220°C and 245°C; die-head temperature is maintained at 230–240°C. Melt temperature below 215°C causes melt fracture and surface roughness at the die lip because plasticized PA12 solidifies rapidly under draw, while sustained melt temperatures above 250°C volatilize the plasticizer and produce die drool, OD drift, and reduced tensile elongation after aging. The extrudate is calibrated by vacuum sizing with closed-loop diameter control using laser gauges reading to ±0.03 mm, then cooled in a two-stage water bath and hauled off at speeds between 30 m/min and 80 m/min depending on OD. Online testing includes spark integrity at 5 kV, dimensional measurement, and batch sampling for burst pressure, low-temperature impact at −40°C, and zinc chloride stress cracking after exposure per SAE J844. Material conformance for export production is documented against SAE J844 and ISO 7628-2:2019, with REACH 1907/2006 and RoHS 2011/65/EU declarations. Terminal products are 6.35 mm to 16.0 mm OD coiled utility lines, bulk reels of 100 m, 200 m, and 500 m, and cut-to-length pre-assembled chassis air harnesses with brass or composite push-in fittings.

    Diesel fuel return lines and vapor-return routing in passenger cars and light commercial vehicles expose the PA12 layer to continuous contact with European diesel fuel at under-hood temperatures between 80°C and 125°C depending on tank proximity and DPF regeneration heat soak. The application requires a specific balance of diesel resistance, low-temperature bendability, and thermo-oxidative stability under continuous wall temperature. Compliance for the finished tubular assembly is documented under SAE J2260, SAE J1737 for permeation testing, and ISO 1817:2015 for resistance to standard test fuels, with REACH and RoHS statements required by vehicle OEM purchasing contracts. In mono-layer diesel return lines, ≥98.0 wt% predried base resin is blended with ≤2.0 wt% carbon black masterbatch and processing aid; plasticizer is not added downstream because the resin is supplied pre-plasticized. In coextruded multi-layer fuel line constructions, VESTAMID® LX9008 is used as the outer PA12 layer or as the inner fuel-contact layer in a five-layer sequence, where the PA12 layers together commonly account for 60–80 wt% of the total wall mass, the EVOH barrier layer accounts for 5–10 wt%, adhesive tie layers account for 8–12 wt%, and the remaining <1 wt% consists of processing stabilizers. Published data for this specific five-layer configuration is limited; exact layer percentages are fixed by permeation testing under SAE J1737 and burst retention after fuel aging. The downstream process is a five-extruder coextrusion line with each screw operating at L/D 24:1 to 30:1, a five-layer spiral mandrel die, and a vacuum calibration tank. Melt temperatures for the PA12 layers are held at 220–240°C, while the EVOH melt is maintained at 190–210°C to limit thermal degradation. Wall-thickness distribution is checked by ultrasonic gauges after the cooling bath; any layer deviation beyond ±0.02 mm from the target layer map triggers automatic rejection because fuel permeation and interlayer adhesion are sensitive to local thinning. The terminal product types include pre-formed diesel return lines with quick-connect terminations, tank-to-filter jumper tubes, fuel vapor purge lines, and bundled fuel line assemblies for Euro 6/VI commercial vehicle platforms. The grade is not recommended for direct continuous contact with biodiesel blends above B20 unless the vehicle OEM has validated the specific compound under ISO 1817 aging at the maximum under-hood temperature.

    Internal Thermoplastic Liner Function in Unbonded Flexible Risers and Flowlines

    In subsea hydrocarbon export and injection lines, the inner polymer liner of an unbonded flexible pipe must resist sour gas permeation, rapid gas decompression damage, and long-term hydrolysis under produced-fluid temperatures between 4°C and 70°C. VESTAMID® LX9008 is applied as the extruded thermoplastic liner layer over the interlocked steel carcass because the plasticized PA12 offers lower flexural modulus than unplasticized PA12 and reduces liner buckling during bending at minimum bend radius. The liner formulation is generally the unblended base polymer: 100 wt% predried virgin pellets are used unless project qualification permits edge-trim regrind at ≤10 wt%; regrind is prohibited in sour-service liners by several operator specifications because hydrolytic degradation history cannot be fully reconstructed. If UV stabilization or color coding is required for topside handling, the additive masterbatch is limited to ≤2.0 wt% and must undergo the same ISO 23936-1:2022 qualification program as the base resin. The extrusion process is performed on a single-screw extruder with L/D 30:1, a barrier screw, and a continuous screen pack of 40/80/100 mesh to remove carbonized gel particles that would create liner defects; melt temperature is controlled to 220–240°C, and the extruder is purged with nitrogen during start-up to limit hydrolytic degradation. The molten tube is drawn over the carcass at haul-off speeds governed by wall-thickness target, usually 4–12 mm depending on pipe diameter and design pressure. After cooling, the liner is tested by ultrasonic thickness mapping, spark integrity at 10 kV/mm wall thickness, and visual inspection for surface gels, contamination, or weld lines. The liner is then sent to the flexible pipe manufacturing line where pressure armor, tensile armor, and outer sheath are wound over it; any liner defect found after armoring cannot be repaired without cutting the entire pipe section.

    Flexible Pipe Liner Compliance Matrix
    StandardScopeVerification Parameter
    API Spec 17JUnbonded flexible pipe systemsDesign pressure, collapse resistance, tensile armor capacity
    ISO 13628-2:2023Subsea unbonded flexible pipeSystem design, manufacturing quality, pressure testing
    ISO 23936-1:2022Non-metallic materials for sour serviceRapid gas decompression, aging, chemical resistance
    NORSOK M-710Non-metallic qualificationSour media compatibility, polymer property retention

    Compliance for the finished unbonded flexible pipe is based on API Spec 17J, ISO 13628-2:2023, ISO 23936-1:2022, and NORSOK M-710, with chemical resistance tested under ISO 1817:2015. The terminal finished products are unbonded flexible risers, flowlines, and jumpers with inner diameters from 50 mm to 500 mm. Operational limitations apply: continuous exposure to produced fluids above 60°C in high-CO₂ gas service can accelerate plasticizer extraction and reduce liner ductility, and exposure to free water with pH below 4 should be prevented during shut-in periods to avoid acid-catalyzed hydrolysis of the PA12 backbone.

    Polyamide 12 pneumatic control tubing used in robotic dress packs, semiconductor clean utilities, and packaging machinery is specified where polyurethane would be too soft and unplasticized PA12 would kink at moving-axis flex points. The formulation is based on 97.0–98.5 wt% predried base resin with 1.5–3.0 wt% blue or black colorant masterbatch; no additional plasticizer or polymer blending is required. Extrusion is carried out on a single-screw tube line with L/D 24:1, internal air calibration, and closed-loop OD control; the melt temperature is held at 220–235°C. The finished tubes, typically 4/6 mm, 6/8 mm, and 8/10 mm OD/wall configurations, are cut to length and assembled into festoon packages or push-in connector-ready coils. Dimensional fits are validated against ISO 14743:2020 for push-in connector compatibility, and material declarations follow REACH and RoHS. The grade is not recommended for continuous use with strong mineral acids or high-aromatic solvent streams; such service requires chemical compatibility testing under ISO 1817:2015.

    When Sheathing Demands Combine Flexibility, Abrasion Resistance, and Halogen-Free Smoke Control

    In automotive sensor cable jacketing, the outer sheath must withstand stone-chip abrasion in wheel arches, repeated flexing at suspension deflection points, and exposure to brake fluid, road salt, and detergent. VESTAMID® LX9008 is compounded for cable extrusion as the base polymer: 85.0–95.0 wt% predried resin is blended with 5.0–15.0 wt% halogen-free flame-retardant masterbatch, 0.5–1.0 wt% processing stabilizer, and 0–2.0 wt% colorant masterbatch; the exact FR loading is set by cable diameter and the flame-propagation requirement of ISO 6722 or the vehicle OEM's LV-class standard. The sheathing process is a pressure-extrusion crosshead on a L/D 25:1 single-screw extruder, with wire preheating at 60–90°C, melt temperature 220–240°C, and a pressure crosshead die to ensure concentric wall thickness of 0.15–0.50 mm. After water cooling and spark testing at 3.0 kV to 5.0 kV, the jacket is checked for concentricity by X-ray or optical diameter gauges; out-of-roundness above 0.05 mm is rejected because it compromises connector sealing. The terminal products are ABS wheel-speed sensor cables, brake wear sensor leads, fuel-pump module wiring jackets, and harness sheathing for engine compartments. Compliance documentation includes ISO 6722, IEC 60754-1:2011, IEC 60754-2:2011, REACH, RoHS, and vehicle-specific requirements for halogen content. The operational boundary is the migration of plasticizers from adjacent PVC insulation: if a PVC primary insulation is used beneath the PA12 sheath, a barrier tape or a non-PVC primary insulation is required to prevent plasticizer migration and jacket embrittlement after heat aging.

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    Certification & Compliance
    More Introduction

    Evonik VESTAMID® LX9008 PA 12 is an aliphatic semi-crystalline polyamide 12 grade supplied for melt extrusion and blow molding. The base polymer is designated PA 12 according to ISO 1043-1. In its standard formulation, the material combines a high-molecular-weight backbone with a heat-stabilization package intended for continuous melt processing at wall temperatures up to 250 °C. Dry-as-molded density determined by ISO 1183-1 is typically 1.01 g/cm³; differential scanning calorimetry under ISO 11357-3 shows a melting endotherm at 175–178 °C. Shore D hardness determined by ISO 7619-1 is typically 70–74. The melt is non-corrosive to standard nitrided barrel steels, but hydrolytic degradation is accelerated when residual moisture exceeds 0.10 % by ISO 15512. Pellets are supplied in moisture-barrier bags and must be dried in a desiccant dryer at 80 °C for 4–6 h when storage humidity has exceeded 60 % RH.

    Within the VESTAMID L series, LX9008 is positioned for high-melt-strength extrusion rather than injection molding. Standard molding grades have a higher melt volume-flow rate under ISO 1133-1 and are preferred for thin-wall parts; the higher molecular weight of LX9008 increases melt stability for parison control but also raises screw torque. Unlike glass-reinforced VESTAMID L-GF30, LX9008 is unfilled and retains elongation at break above 250 % under ISO 527-2. Notched Charpy impact energy at 23 °C is typically 14–18 kJ/m² and at −30 °C is 6–8 kJ/m² under ISO 179-1/1eA. The saturated moisture regain of PA 12 is approximately 1.4–1.6 % by immersion in water at 23 °C per ISO 62, contrasting with PA 6 saturation values near 9–10 %.

    Moisture uptake follows Fickian behavior at thin sections. At 23 °C and 50 % RH, a 1 mm plaque reaches a practical moisture plateau within 24–48 h; a 4 mm extruded tube wall requires 72–120 h to reach 0.5 % moisture. If pellets are dried to below 0.10 % but held in an open hopper at 60 % RH, surface moisture can rise to 0.20 % within 2 h. This absorbed moisture lowers the melt viscosity and can create surface splay in thick profiles. Closed-conveying systems with hopper dryers are therefore used on continuous extrusion lines.

    What Restricts the Melt-Temperature Window in Long-Residence Extrusion?

    Thermal degradation in PA 12 is governed by residence time and oxygen ingress at the feed throat. Published extrusion guidelines for VESTAMID PA 12 specify barrel temperature profiles between 220 °C and 250 °C, with the die head not exceeding 240 °C for tube wall thicknesses below 1.5 mm. Melt temperature measured by an immersed thermocouple at the die entry should be maintained below 260 °C; excursions above 280 °C produce measurable viscosity loss, discoloration, and surface defects. On a 30 L/D single-screw extruder with a barrier screw and 3:1 compression ratio, stable melt pressure between 120 bar and 180 bar is typical for 8 mm to 16 mm tubing. The feed zone is set at 40–60 °C to prevent pellet bridging, while hopper magnets and fine screen packs of 60/80 mesh reduce carbonized gels. Because PA 12 is semicrystalline, the screw design must provide sufficient energy to melt the crystalline fraction without generating excessive shear. Use of temperature overrides to compensate for high melt viscosity is not recommended; instead, screw speed is lowered or barrel profile is adjusted to keep adiabatic melt rise within 10 °C. Extruder start-up following a material change from PA 6 requires purging with a low-MFR polyolefin or acrylic purging compound; direct transition from PA 6 without purging can generate incompatible phases and black specks. Barrel temperatures are reduced by 20–30 °C when shutting down for more than 30 min to limit thermal history. Residence time at melt temperatures above 250 °C should be kept below 15 min. Degraded PA 12 shows a characteristic increase in die head pressure fluctuation and a reduction in Charpy notched impact energy before visible discoloration.

    Compressed-air brake tubing produced from LX9008 is evaluated under SAE J844 and ISO 7628. In commercial practice, coextrusion of 12 mm OD × 8 mm ID polyamide 12 tubing uses an outer LX9008 layer and, where static dissipation is required, an inner conductive PA 12 layer. Vacuum sizing at −0.2 bar to −0.4 bar and a water bath temperature of 12–18 °C are typical. Post-extrusion conditioning at 90 °C in a hot-water bath for 2 h stabilizes crystalline morphology and reduces longitudinal shrinkage below 2 % when tested at 150 °C for 1 h. Burst pressure at 23 °C for this geometry typically exceeds 40 bar; after 1,000 h at 100 °C in circulating air, burst retention above 70 % is expected. This distinguishes PA 12 from PA 6, which loses more tensile strength in hot-wet environments due to absorption-driven plasticization and hydrolysis.

    Comparative Water Absorption and Low-Temperature Impact Across Polyamide Families

    The selection of PA 12 over PA 6 or PA 66 in under-hood and pneumatic systems is justified by property retention after moisture conditioning. The table below summarizes typical values drawn from published polyamide data and manufacturer datasheets; exact batch specifications for VESTAMID LX9008 should be obtained from the supplier.

    Property Unit Method VESTAMID LX9008 Unplasticised PA 12 PA 11 PA 66
    Density g/cm³ ISO 1183-1 1.01 1.01–1.02 1.03–1.04 1.13–1.14
    Melt temperature °C ISO 11357-3 175–178 175–182 187–192 255–265
    Water absorption at 50 % RH % ISO 62 0.7–0.8 0.7–0.8 1.0–1.2 2.5–3.0
    Water saturation in water at 23 °C % ISO 62 1.4–1.6 1.4–1.6 1.8–2.0 8.0–9.0
    Charpy notched impact at −30 °C kJ/m² ISO 179-1/1eA 6–8 5–8 7–9 3–5
    Tensile modulus MPa ISO 527-2 1200–1400 1300–1500 1000–1300 2900–3200

    The lower saturated moisture uptake of PA 12 is a direct consequence of the lower amide group density relative to PA 6 and PA 66. This preserves tensile modulus and flexural modulus after exposure to condensing humidity. At −30 °C, the notched impact behavior of LX9008 approaches that of PA 11, while the density remains lower. PA 66 offers higher short-term strength and heat resistance but is more sensitive to glycol-based coolants and hot-water hydrolysis; PA 12 is specified where long-term chemical exposure and low-temperature flexibility outweigh maximum dry tensile strength.

    Flexible liners for offshore umbilicals and cable sheathing are a second application scenario. In these applications, long-chain aliphatic polyamides are selected because hydrocarbon resistance and hydrolysis resistance reduce stress cracking in the presence of methanol, glycol, and salt water. LX9008 is processed into tube profiles that are spiral-wrapped or co-extruded with high-density polyethylene. The PA 12 layer provides barrier and abrasion resistance; the HDPE layer contributes moisture isolation and cost reduction. Adhesion is promoted by maleic anhydride-grafted tie resins at 2–5 % by mass. In salt-spray testing to ISO 9227 NSS, PA 12 retains tensile elongation after 1,000 h exposure better than PA 6, although published data for this specific multi-layer configuration is limited. The material should not be processed with flame-retardant masterbatches based on ammonium polyphosphate unless pre-drying and melt temperature are re-qualified, because acid generation can catalyze polyamide chain scission.

    Connectors and fittings are often injection molded from lower-viscosity PA 12 grades; LX9008 is not optimized for thin-wall injection molding because its high melt viscosity requires higher filling pressure and risks short shots below 0.8 mm wall thickness. When used in fittings, melt temperature should be 240–260 °C, mold temperature 40–60 °C, and holding pressure 600–900 bar. Gate dimensions should be 50–80 % of part thickness to avoid jetting.

    When PA 12 Replaces PA 6 or PA 66 in Cyclic Humidity Service

    In environments where relative humidity cycles between 20 % and 85 %, PA 6 and PA 66 absorb and desorb moisture over a 24–72 h period, causing dimensional change. PA 12 at 50 % RH exhibits moisture absorption of approximately 0.7 % and post-molding moisture expansion of approximately 0.1 % per 1 % water uptake, compared with PA 6 grades that can show 0.6 % length change between dry and saturated states. This makes PA 12 suited for precision pneumatic fittings and industrial quick-connects. However, the thermal limit is lower: continuous service temperature of PA 12 in air is typically specified at 80–100 °C, whereas unfilled PA 66 parts may sustain 120–140 °C. This boundary must be compared with hot-oil or hot-water exposure. In circulating hot air at 150 °C, oxidative embrittlement occurs after hundreds of hours; the heat stabilization package in LX9008 shifts the failure threshold but does not eliminate it.

    Regulatory Verification Requires Grade-Specific Certification

    Compliance statements for VESTAMID LX9008 must be verified against the certificate of analysis. Polyamide 12 base resins may be evaluated under FDA 21 CFR 177.1500 for food-contact components and are commonly supplied under a REACH registration pursuant to Regulation (EC) No 1907/2006. RoHS compliance is typically limited to the four heavy metals and does not extend to all flame-retardant additives unless explicitly certified. The product is not recommended for prolonged immersion in hot concentrated mineral acids, phenols, or formic acid at temperatures above 50 °C. Storage should be in unopened, moisture-barrier bags below 60 % RH; once opened, the material should be resealed with desiccant and processed within 24 h or re-dried.

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