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Evonik VESTAMID eCO LX9039 BBM100 Nylon 12, Dry

    • Product Name: Evonik VESTAMID eCO LX9039 BBM100 Nylon 12, Dry
    • Factroy Site: Yudu County, Ganzhou, Jiangxi, China
    • Price Inquiry: admin@ascent-chem.com
    • Manufacturer: Ascent Petrochem Holdings Co., Limited
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    Specifications
    HS Code 794090
    Density Dry 1.01 g/cm³
    Water Absorption 24h 0.2%
    Tensile Modulus Dry 1600 MPa
    Yield Stress Dry 45 MPa
    Nominal Strain At Break Dry 200%
    Charpy Notched Impact Strength At 23 C Dry 10 kJ/m²
    Charpy Notched Impact Strength At 30 C Dry 5 kJ/m²
    Melting Point Dsc 178 °C
    Glass Transition Temperature Dry 53 °C
    Vicat Softening Temperature B50 145 °C
    Heat Deflection Temperature At 0 45 Mpa 90 °C
    Heat Deflection Temperature At 1 80 Mpa 50 °C

    As an accredited Evonik VESTAMID eCO LX9039 BBM100 Nylon 12, Dry factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing Evonik VESTAMID eCO LX9039 BBM100 Nylon 12, Dry is packaged in 25 kg moisture-proof sealed bags, nitrogen-blanketed, ready for use.
    Container Loading (20′ FCL) 20′ FCL: Dry nylon 12 granules packed in sealed bags on pallets, securely loaded for safe transport.
    Shipping VESTAMID eCO LX9039 BBM100 Nylon 12 ships in sealed, moisture-proof packaging to preserve dryness. Palletized, labeled, and transported via standard freight. Avoid exposure to humidity, rain, or direct sunlight. Handle with care to prevent bag damage. Not classified as dangerous goods under normal transport conditions.
    Storage Store Evonik VESTAMID eCO LX9039 BBM100 Nylon 12 (Dry) in its original, tightly sealed container in a cool, dry, well-ventilated area. Protect from moisture, direct sunlight, and heat sources. Ideal storage temperature is below 30°C (86°F). Ensure containers remain sealed when not in use to prevent moisture pickup.
    Shelf Life Store in original sealed packaging, cool and dry. Shelf life is typically two years from manufacture date for this Nylon 12.
    Application of Evonik VESTAMID eCO LX9039 BBM100 Nylon 12, Dry

    VESTAMID eCO LX9039 BBM100 dry is a plasticized polyamide 12 grade supplied under mass balance certification; the eCO designation does not alter the polymer backbone. Application scenarios below are restricted to downstream extrusion of cable sheathing, conduit, tube, and profile products where low moisture regain, low-temperature impact, and halogen-free behaviour are specified. Process settings are reported from production-scale single-screw lines and are adjusted by a site-specific process capability study.

    In automotive engine bay corrugated conduit extrusion, VESTAMID eCO LX9039 BBM100 dry is fed from a desiccant dryer maintaining a dew point of -40 °C or lower into a 45 mm single-screw extruder with 30:1 L/D and a grooved feed zone. Residual moisture is kept below 0.10 wt% as determined by ISO 15512 Method B on a hopper sample; exposure to ambient air above 60 % relative humidity for more than 30 min requires re-drying at 80 °C for 4 h to 6 h. The barrel profile is normally set from 190 °C in zone 1 to 225 °C at the die; melt pressure before the breaker plate is observed between 90 bar and 140 bar on a 3-zone screw with a shallow metering section. A vacuum vent of -0.8 bar is applied after the melting zone to remove residual moisture and plasticizer volatiles that otherwise create pinholes in the corrugator. The BBM100 designation indicates black pigmentation, so no additional carbon black masterbatch is added. The melt enters a vacuum corrugator with forming blocks calibrated to an internal diameter of 7.5 mm to 40 mm; wall thickness is held between 0.3 mm and 0.7 mm. In production-scale trials, pressure fluctuation at the die above 5 bar during a 30 min run correlates with intermittent block filling and ovality greater than 3.0 %. The finished corrugated conduit is tested in accordance with LV 312-1 for protective conduit systems; abrasion resistance is evaluated using the method referenced in ISO 6722-1, and low-temperature impact is checked at -40 °C. The extrusion grade is halogen-free and does not release acid gases under IEC 60754-1, but it is not classified as flame-retardant and should not be specified where a V0 classification is required without an additional FR jacket.

    What Limits Line Speed Before Melt Fracture Appears in Thin-Wall Category 6A Sheathing?

    High-speed sheathing of Category 6A industrial Ethernet cable uses a 50 mm single-screw extruder with 30:1 L/D and a pressure crosshead. The dry granulate is not exposed to ambient air for more than 15 min; dried resin moisture is held below 0.08 wt% due the thin wall of 0.15 mm to 0.35 mm. Barrel temperatures are kept low in the feed section at 185 °C and increased to 220 °C at the head. The limiting parameter is melt fracture at the die land; when wall shear rate is calculated from die land dimensions and volume throughput, values above 1,000 s⁻¹ initiate sharkskin in plasticized PA12 unless die temperature is raised in 5 °C increments. Production data show that line speed can be increased from 150 m/min to 300 m/min only if melt pressure at the crosshead remains below 180 bar and the melt pump suction side is kept at 20 bar to 30 bar.

    Melt volume-flow rate is measured per ISO 1133-1 at 230 °C under 5 kg; batch-to-batch variation outside the converter-accepted range leads to non-concentric wall distribution and sheath ovality. The cable core is preheated to 60 °C to 80 °C before crosshead entry to reduce shrinkage mismatch. The sheathed cable is tested for tensile elongation per IEC 60811-501, flame retardancy per IEC 60332-1-2, and halogen acid gas absence per IEC 60754-1. Typical final constructions are four-pair Category 6A cables with outer diameter 6.5 mm to 8.0 mm used in robotic dress packs and machine-tool cable carriers; torsional stress of ±180°/m and bending radius down to 7.5 × OD are end-use tests. The plasticized PA12 sheath should not be specified as the sole fire barrier for CPR Euroclass B2ca or higher; an additional intumescent layer is required when the cable is routed through spaces governed by EN 50575.

    When Pneumatic Control Lines Replace PA11 in Heavy-Duty Vehicle Air Brake Circuits

    SAE J844 air brake tubing in heavy-duty vehicles is extruded from VESTAMID eCO LX9039 BBM100 dry as a single-layer tube with outer diameter 6.35 mm and inner diameter 4.0 mm, although other sizes to 16 mm OD are produced. The tube is vacuum-sized after a 45 mm extruder with 30:1 L/D and a mixing screw containing a dispersion section; melt temperature at the die is limited to 210 °C to 220 °C to avoid plasticizer volatilization that shows as internal haze. Drying uses a dew point of -40 °C and a moisture target below 0.10 wt%; regrind from post-industrial tube scrap is limited to 20 wt% because higher levels reduce burst strength after 72 h at 100 °C heat ageing. Compared with PA11, the PA12 backbone yields a lower equilibrium moisture uptake in humid air; this reduces post-installation OD growth and fitting leak risk in compressed air circuits.

    The extruded tube must hold an OD tolerance of ±0.05 mm to ensure collar retention on push-to-connect fittings. Burst pressure at room temperature is tested according to SAE J844 and is typically not less than 4 × the working pressure of 1.0 MPa for 6.35 mm × 4.0 mm tube; low-temperature impact is checked at -40 °C per ISO 7628-1. The plasticized PA12 formulation provides resistance to compressor oil and zinc chloride road de-icing solutions, but continuous use above 110 °C at the tube surface shortens stabilizer life. Final applications are air brake circuits, suspension levelling lines, and transmission shift lines on trucks and trailers where SAE J844 type A construction is approved.

    In railway rolling stock cable jacketing, the outer sheath is pressure-extruded over a twisted core containing crosslinked elastomer-insulated conductors and a metallic screen; the PA12 melt must not exceed 230 °C at the crosshead because higher temperatures shrink the elastomer insulation and create voids. The extruder is typically a 60 mm single-screw unit with 30:1 L/D and a barrier screw; drying to 0.08 wt% moisture is verified by ISO 15512. A melt pump is used to reduce pressure pulsations; crosshead pressure is maintained between 120 bar and 160 bar. The cable jacket wall thickness is set from 0.6 mm to 1.2 mm depending on cable outer diameter. The outer sheath is required to pass low-temperature impact at -40 °C per EN 60811-506, oil immersion at 100 °C for 168 h per EN 60811-404, and halogen acid determination per IEC 60754-1. The eCO mass balance feedstock is tracked by ISCC PLUS certification; the polymer backbone is chemically equivalent to fossil-based PA12, so existing process settings do not change.

    Rolling stock cables built with this sheath are generally assessed under EN 50264-1 for construction and EN 45545-2 for fire performance. The PA12 layer contributes low smoke and halogen-free behaviour but does not by itself achieve HL3 without additional fire barrier tapes or ceramifiable elastomer inner layers. Production experience shows that moisture regain in silo storage above 0.12 wt% before extrusion produces surface roughness on the cable jacket, and a re-drying cycle of 80 °C for 5 h is required before resuming line speed above 25 m/min.

    Downstream segmentCritical processing windowPrimary standardsEnd-use threshold
    Automotive corrugated conduitMoisture 0.10 wt% max; die 225 °C maxLV 312-1, ISO 6722-1Ovality 3.0 % max; impact -40 °C
    Category 6A cable sheathingShear rate 1,000 s⁻¹ max; melt pump suction 20 bar to 30 barIEC 61156-6, IEC 60332-1-2Tensile elongation per IEC 60811-501
    Air brake tubingOD tolerance ±0.05 mm; regrind 20 wt% maxSAE J844, ISO 7628-1Burst 4 × working pressure; impact -40 °C
    Railway cable jacketCrosshead 230 °C max; moisture 0.08 wt% maxEN 50264-1, EN 45545-2Oil ageing 168 h at 100 °C; impact -40 °C
    Spiral wrap and scuff sleeveCalibrator water 15 °C to 20 °C; regrind 15 wt% maxISO 6945, IEC 60754-1Mandrel bend -40 °C; shrinkage 2.0 % max
    Subsea control line sheathPreheat 120 °C to 150 °C; line speed 5 m/min to 15 m/minAPI 17E, ASTM D746Brittleness -40 °C; adhesion per ASTM D4541

    Spiral Wrap and Hydraulic Hose Scuff Sleeving

    Spiral wrap for mobile machinery is profile-extruded through a 40 mm single-screw extruder with 24:1 L/D; the screw has a shallow metering section because the plasticized PA12 melt is more sensitive to residence time than unplasticized PA12. Drying follows the same -40 °C dew point and 0.10 wt% moisture ceiling. The profile die is held at 200 °C to 210 °C, and the cooling calibrator uses water at 15 °C to 20 °C; this narrow temperature differential is kept below 25 °C to prevent spiral pitch distortion after cutting. Post-industrial regrind is incorporated at 15 wt% maximum because higher regrind levels raise melt viscosity and alter the spiral pitch.

    Hydraulic hose scuff sleeves are cut from the same extrudate in lengths matching hose outer diameters from 10 mm to 50 mm. Abrasion resistance is evaluated against ISO 6945, and low-temperature flexibility is checked after 24 h at -40 °C by winding the sleeve around a mandrel equal to the hose OD. The product is halogen-free per IEC 60754-1 and provides a scuff barrier between hose cover and adjacent metal edges; it is not intended for fluid containment and does not replace the hose reinforcement. Continuous surface temperature should be limited to 100 °C; excursions above 125 °C lead to longitudinal shrinkage above 2.0 % in production audits.

    For subsea hydraulic control lines, the outer PA12 sheath is applied by crosshead extrusion over a 316L stainless steel tube preheated to 120 °C to 150 °C before entering the die; this preheat prevents skin solidification and delamination. The line speed is limited to 5 m/min to 15 m/min because the wall thickness varies from 1.0 mm to 2.5 mm and cooling must be uniform to avoid residual stress. Drying is identical to other applications, with moisture below 0.08 wt% because the thicker sheath magnifies void formation from steam. The extruder is a 50 mm unit with 30:1 L/D and a melt pump; melt temperature is held at 215 °C to 225 °C. The sheath is tested for adhesion by ASTM D4541 pull-off, low-temperature brittleness per ASTM D746 at -40 °C, and immersion in methanol/water mixtures according to API 17E guidance. Published data for this specific configuration is limited; therefore production acceptance is performed on a line-by-line basis against a qualified field sample.

    The final product is used as an outer protective layer in subsea umbilical control lines and chemical injection jumpers, where seawater, hydraulic fluid, and methanol exposure occur simultaneously. The sheath is not a primary pressure barrier and must not be specified for gas-carrying riser service without a full API 17E qualification program. The ISCC PLUS mass balance certificate links the eCO feedstock to the finished sheath batch, but the mechanical datasheet of the compound is unchanged from fossil-based LX9039.

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    Certification & Compliance
    More Introduction

    Evonik VESTAMID eCO LX9039 BBM100 Nylon 12, Dry is a black-pigmented polyamide 12 powder supplied in moisture-controlled packaging for laser powder bed fusion. The “eCO” designation identifies an ISCC PLUS mass-balanced allocation of renewable feedstock in the polyamide 12 value chain; the polymer backbone remains chemically identical to fossil-derived VESTAMID LX9039, and the “Dry” suffix denotes a low as-packed moisture condition rather than a separate chemical grade. The powder is processed on CO₂ laser systems operating at 10.6 µm wavelength and is positioned as a drop-in material where current fossil PA12 powders are already qualified.

    Does the mass-balanced eCO ledger alter crystallization or laser energy requirements?

    Mass-balanced feedstock allocation does not alter the PA12 macromolecular structure, and therefore the thermal transitions relevant to powder bed fusion remain governed by the same semi-crystalline morphology as the fossil reference. The supplier’s current technical datasheet lists a melting peak by ISO 11357-3 in the region of 176 °C. Industrial build beds are typically held between 168 °C and 178 °C, but the final setpoint is machine-specific and is affected by part packing density, build envelope insulation, and IR pyrometer emissivity settings. Because the black pigment modifies laser energy absorption at 10.6 µm, parameters validated for unfilled natural PA12 should not be transferred directly. A calibration matrix varying laser power, scan speed, and beam offset should be used to establish the sintering window for the target machine. Published data for this specific configuration is limited; however, production experience with equivalent black PA12 grades indicates that part density stabilizes when the energy input is sufficient to produce a fully molten track without over-sintering the surrounding bed.

    Powder bed fusion performance is determined initially by particle size distribution and bulk packing. VESTAMID eCO LX9039 BBM100 is supplied as a dry, free-flowing powder with a typical particle size distribution centered near 55 µm when measured by laser diffraction according to ISO 13320-1. Bulk density determined by ISO 60 is approximately 0.45 g/cm³. The particle shape is controlled by the precipitation process used for VESTAMID PA12 powders, and the grade is designed for consistent recoating on blade and counter-rotating roller systems. Table 1 summarizes typical powder characteristics reported in the technical datasheet.

    PropertyTest standardUnitTypical value
    Bulk densityISO 60g/cm³0.45
    Particle size D50ISO 13320-1µm55
    Melting pointISO 11357-3°C176
    As-packed moistureISO 15512% by mass≤0.10

    Mechanical characterization of laser-sintered test specimens is performed under ISO 527-2 for tensile properties and ISO 179-1 for Charpy impact. The typical datasheet values for sintered parts include a tensile modulus in the range of 1500 MPa and tensile strength near 45 MPa; elongation at break is generally reported near 20 %. The material exhibits the layer-wise anisotropy common to powder bed fusion PA12, and Z-direction strength is typically lower than XY-plane values. Users validating this grade for load-bearing applications should include specimens oriented in XY, XZ, and Z build directions, and should not rely only on datasheet values generated from optimized XY-oriented test bars. Table 2 lists representative mechanical and thermal property values.

    PropertyTest standardUnitTypical value
    Sintered part densityISO 1183-1g/cm³1.01
    Tensile modulusISO 527-2MPa1500
    Tensile strengthISO 527-2MPa45
    Elongation at breakISO 527-2%20
    Flexural modulusISO 178MPa1400
    Notched Charpy impactISO 179-1kJ/m²4.5
    Heat deflection temperature BISO 75-2°C150

    When moisture exceeds 0.1 % by weight, drying becomes a processing prerequisite

    Moisture is a critical variable in PA12 powder handling. Although PA12 absorbs less water than short-chain polyamides, powders exposed to ambient humidity can reach moisture levels that cause steam generation at the laser melt front. The symptom is surface pitting, excessive porosity, and reduced tensile elongation. For VESTAMID eCO LX9039 BBM100, the as-packed moisture is controlled, but opened bags should be sealed immediately after material withdrawal. If powder has been exposed for more than 1 h at relative humidity above 60 %, pre-drying is recommended. The powder should be dried in a dry-air oven at 80 °C for 4 h to 6 h, at a bed depth not exceeding 5 cm. After drying, the material should be cooled to below 40 °C in a sealed container before sieving and loading. Conveying systems should use dried compressed air or nitrogen to avoid reintroducing moisture during transfer.

    Failure to manage moisture may not be immediately visible in green parts, but the reduction in melt viscosity at the laser interaction zone can create inconsistent layer fusion and localized porosity that appears only after dye infiltration or mechanical testing.

    Batch-to-batch variation on production laser sintering lines has been minimized through tight powder specification control, but recycled powder aging remains an operational boundary. In standard PA12 powder bed fusion, used powder is mixed with virgin material at a refresh rate typically between 30 % and 50 % by mass. Below that range, repeated thermal exposure shifts the molecular weight and widens the crystallization window, producing rough side surfaces and a measurable drop in elongation at break. The eCO grade should be treated with the same powder management protocol as fossil-derived VESTAMID LX9039; no additional refresh-rate advantage is specified in the current datasheet. When changing powder lots, build parameters should be requalified with a short build environment verification, and the used-powder fraction should be sieved through a 250 µm mesh to remove sintered agglomerates and contamination.

    VESTAMID eCO LX9039 BBM100 relative to other PA12 and bio-based powders

    The primary difference from conventional VESTAMID LX9039 BBM100 is the mass-balanced renewable feedstock allocation. The eCO grade carries a lower cradle-to-gate carbon footprint and is supported by ISCC PLUS certification, while the polymer chemistry, melting point, and processing window are positioned as equivalent to the fossil reference. Compared with natural unfilled PA12 powders, the black pigmentation modifies laser absorption and may require different process parameters; it also provides uniform dark part color without a secondary dyeing step. Compared with glass-bead-filled PA12 powders, VESTAMID eCO LX9039 BBM100 delivers higher elongation at break and lower modulus, making it less suitable for stiff jigs and fixtures but more suitable for snap-fit and hinge-type components. Compared with PA11 powders derived directly from castor oil, the eCO PA12 grade is not a chemically different polymer; it is a mass-balanced PA12 and therefore retains the lower water absorption and established PA12 service behavior of the VESTAMID platform.

    The product is used in functional prototypes, series-production housings, ducts, brackets, and consumer goods where PA12’s combination of chemical resistance, impact resistance, and low water absorption is required. End-use qualification for medical or food-contact applications must be performed against the relevant regulatory standard such as ISO 10993 for medical devices or FDA 21 CFR 177.1500 for nylon resins, and the supplier’s grade-specific compliance statement should be obtained. The powder should not be blended with glass-filled or other polymer powders unless compatibility and segregation behavior have been validated, because differences in particle density and surface chemistry can create layer defects and anisotropic property loss.

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