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EMS-Grivory Grilamid LV-3H Nylon 12, 30% Glass Fiber Filled, Conditioned

    • Product Name: EMS-Grivory Grilamid LV-3H Nylon 12, 30% Glass Fiber Filled, Conditioned
    • Factroy Site: Yudu County, Ganzhou, Jiangxi, China
    • Price Inquiry: admin@ascent-chem.com
    • Manufacturer: Ascent Petrochem Holdings Co., Limited
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    Specifications
    HS Code 297511
    Density 1.23 g/cm³
    Glass Fiber Content 30 %
    Water Absorption 24h 0.3 %
    Tensile Strength Break Conditioned 100 MPa
    Tensile Modulus Conditioned 5000 MPa
    Elongation At Break 4 %
    Flexural Modulus Conditioned 4300 MPa
    Charpy Impact Notched 23 C Conditioned 10 kJ/m²
    Melting Point 178 °C
    Heat Deflection Temperature 0 45 Mpa 175 °C
    Heat Deflection Temperature 1 80 Mpa 170 °C

    As an accredited EMS-Grivory Grilamid LV-3H Nylon 12, 30% Glass Fiber Filled, Conditioned factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing Packaged as 25 kg net in moisture-proof, polyethylene-lined paper bags, palletized and stretch-wrapped for protection.
    Container Loading (20′ FCL) 20′ FCL loading: palletized bags of Grilamid LV-3H nylon 12, 30% glass-filled, conditioned, securely stowed for safe transport.
    Shipping Grilamid LV-3H nylon 12 (30% glass fiber) ships as conditioned pellets in sealed, moisture-proof bags or drums to preserve low moisture content. Store in a dry area below 50°C. Standard freight is suitable; avoid excessive heat, humidity, and puncturing packaging during handling and transit.
    Storage Store Grilamid LV-3H in its original, sealed container in a cool, dry, well-ventilated area. Protect from moisture absorption, direct sunlight, and high heat. Keep away from sources of ignition and incompatible chemicals. Maintain moderate humidity to prevent condensation. Properly sealed storage preserves the conditioned nylon's properties; avoid prolonged storage under humid or extreme conditions.
    Shelf Life Shelf life is typically 2-3 years from shipment if stored in original unopened packaging in a dry, cool area.
    Application of EMS-Grivory Grilamid LV-3H Nylon 12, 30% Glass Fiber Filled, Conditioned
    In compressed-air brake systems, the coupling bodies and relay valve end covers are injection-moulded from Grilamid LV-3H in the conditioned state with 30 wt% short-glass-fibre reinforcement. The pellet bed is pre-dried at 80 °C for 4 h to 6 h in a desiccant dryer with a supply-air dew point below -30 °C, producing residual moisture below 0.10 wt%. Barrel temperatures are set from 60 °C at the throat to 230 °C in the metering zone and 245 °C at the nozzle. Mould temperature is held between 60 °C and 80 °C. Pressure-boundary components are run with 0–15 wt% regrind. The external release collar may accept up to 20 wt% regrind when the regrind is from the same lot, dust-free and re-dried to the same moisture condition. Dimensional acceptance for commercial-vehicle air-brake circuits references ISO 7628-1:2010 and SAE J844. The terminal parts include push-in collet bodies, threaded adaptors and relay-valve end covers. In collet arms below 1.0 mm wall thickness, glass fibre orientates along the flow direction and creates a weak interface at the melt convergence. Injection speed is increased and melt temperature is set at the upper end of the window only when the flow length-to-thickness ratio exceeds 200:1. A cold slug at the collet hinge can create a visible flow halo and reduce pressure retention. That defect is the main production bottleneck on fastener-feed moulds with narrow gate land lengths.

    What Limits the Permitted Regrind Fraction in Pneumatic Quick-Release Couplings?

    Industrial pneumatic quick-release couplings made from the conditioned grade are assembled into compressed-air systems designed according to ISO 4414:2010. Interchangeability is checked under ISO 6150. The glass-fibre fraction is fixed at 30 wt% by the grade specification. Any dilution or glass-content shift on the threaded pressure boundary is not accepted because it changes creep resistance and burst-pressure scatter. Regrind fraction for the release sleeve can be 25 wt% if the regrind is dry, pellet-uniform and free of fines. For the threaded body, regrind is limited to 10 wt%. Above that limit, repeated extrusion shortens glass-fibre length and widens burst-pressure variance. Melt temperature is held at 230 °C to 250 °C. Mould temperature is 60 °C to 80 °C. Back pressure is set at 0.5 MPa to 1.0 MPa. Hold pressure is maintained at 80 MPa to 100 MPa until gate freeze. Assemblies are cycled for 10,000 connect/disconnect operations at 10 bar and 60 °C. The finished products are push-in fittings, shut-off plugs and angled flow restrictors. A failure mode is stress cracking at the thread root after exposure to phosphate-ester compressor-oil mist. For this reason, the grade is not accepted where oil mist carries more than 5 wt% ester lubricant unless the fitting is specified only for filtered air.Where fuel vapours and road de-icing agents condense on underhood hardware, clip retention force and bracket creep become the controlling design factors. Grilamid LV-3H is processed with the same drying profile: 80 °C for 4–6 h until residual moisture is below 0.10 wt%. The 30 wt% glass-fibre content supplies sufficient bending stiffness to keep clip retention force above the detachment threshold after thermal ageing. Chemical-resistance validation runs according to ISO 16750-5:2010 using reference liquids from ISO 1817 at 23 °C for 72 h. The terminal parts include fuel-line clip assemblies, urea-tank bracket arms and vapour-canister mounting brackets. Mould temperature is held at 80 °C to 100 °C to reduce shrinkage differential between the glass-rich skin and the unreinforced core. In ribbed support arms, a mould temperature below 70 °C increases post-mould warpage beyond 0.3 mm across 100 mm length. The operating boundary is 80 °C continuous in fuel contact. Above that temperature, PA12 creep under clamp load may permit clamp-force relaxation. Regrind is limited to 15 wt%. A production bottleneck is masterbatch incompatibility. A polyolefin-based colour masterbatch above 2 wt% produces delamination at the gate area and lowers short-beam strength. Only polyamide-12-based masterbatch is used, pre-dried, with carrier resin restricted to 1–2 wt%.

    Impact Behaviour of Marine Cable Gland Housings at -25 °C

    Marine and industrial cable glands use the conditioned grade for threaded housings, locknuts and clamping inserts. The relevant standard for cable glands is IEC 62444:2010. Ingress protection is specified under IEC 60529. The moulding process uses a melt temperature of 230 °C to 250 °C and a mould temperature of 80 °C to 100 °C because the higher tool temperature improves thread-shape replication and reduces brittle failure at -25 °C. The 30 wt% glass-fibre filler increases tensile stiffness, but it also creates notch sensitivity at the thread root. In moulding trials, a mould temperature of 60 °C produced a higher frequency of thread-root cracking during cold impact. The remedy is to widen the thread-root radius above 0.4 mm and locate the gate away from the thread face. Regrind content is restricted to 20 wt% for non-flame-rated glands. If RoHS compliance is required, the supplier documents that the glass-fibre sizing and heat-stabiliser package meet Directive 2011/65/EU Annex II limits for lead, mercury, cadmium, hexavalent chromium, PBB and PBDE. The finished parts include IP68 compression glands and EMC-type shield glands. The material is not used where a V-0 flame rating is mandatory. Grilamid LV-3H is typically classed HB under UL 94, and thin-wall flame performance must be verified on the final housing. This is an operational limit rather than a processing failure.Steam sterilisation of reusable handheld instruments imposes repeated moisture exposure, thermal cycling and loaded dimensional checks. Grilamid LV-3H is dried to below 0.10 wt% moisture and then moulded at a melt temperature of 230 °C to 250 °C with the mould at 80 °C to 100 °C. The 30 wt% glass-fibre content reduces thermal expansion and improves structural stiffness after repeated autoclave exposure. Validation is performed on the finished device because raw-material data cannot replace biocompatibility evaluation. Cytotoxicity screening follows ISO 10993-5:2009. Irritation and sensitisation are addressed under ISO 10993-10:2010. Moist-heat sterilisation is run at 134 °C for 3 min per ISO 17665-1:2006 for 100 cycles. The terminal products are sterilisation trays, reusable hand-instrument handles and housing shells for diagnostic cameras. Post-sterilisation dimensional change is controlled by conditioning moulded parts at 23 °C/50 % RH for 48 h before final gauging. The operational boundary is that PA12 is not a replacement for polyphenylsulfone at continuous steam exposure above 150 °C. For this grade, 134 °C intermittent exposure is acceptable only when the applied load is below the creep limit. Published data for Grilamid LV-3H in repeated autoclave use is limited, so cycle-specific device data must be generated. Regrind is not permitted in this segment unless the device specification allows post-industrial reprocessing under ISO 10993-1:2018 risk assessment.

    Power Tool Gear Case Weld Lines Are Assessed Before Drop Testing

    Battery-powered hand tools use the conditioned grade for structural gear-case halves and handle frames. The finished products are tested to IEC 62841-1:2014. Critical geometry includes deep pockets, boss towers and rib junctions. The 30 wt% glass-fibre fraction increases injection-pressure demand. The melt temperature is 230 °C to 250 °C. The mould temperature is 80 °C to 100 °C. Fill time is kept below 1.5 s for thin-walled ribs to avoid premature freeze-off. The principal failure mode is weld-line cracking in the gear case at the junction behind the motor-mount boss. In short-shot trials, the weld line appears as a visible cold line and produces a notch-sensitive region. Sequential valve gating or overflow tabs are used to move the weld line into a low-stress web. Regrind fraction is limited to 15 wt% because higher regrind shortens glass-fibre length and widens weld-line property scatter. After moulding, parts are moisture conditioned to equilibrium at 23 °C/50 % RH before drop testing. The boundary condition is repeated impact after conditioning. Un-conditioned dry parts show higher stiffness but lower elongation. If the tool is specified for outdoor use, low-temperature drop testing at -10 °C is required. When the product standard does not specify this test, room-temperature data must not be extrapolated to cold-impact performance.
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    Certification & Compliance
    More Introduction

    Within the EMS-Grivory polyamide 12 range, Grilamid LV-3H is documented by the manufacturer as a 30% glass fibre reinforced injection moulding compound based on PA12. The product descriptor “Conditioned” refers to test data generated after moisture equilibrium under ISO 1110:2019, typically at 23°C and 50% RH, rather than the dry-as-moulded state. The grade is positioned for load-bearing injection-moulded components that require a balance of stiffness, low moisture uptake, chemical resistance, and post-moulding dimensional stability. Compared with unreinforced PA12 grades, the addition of 30% short glass fibres raises tensile and flexural modulus while reducing elongation at break. Compared with PA66-GF30 and PA6-GF30, the PA12 matrix in LV-3H absorbs less moisture, producing a smaller modulus shift between dry and humid service and lower hygroscopic swelling. The grade is referenced in technical literature for thin-wall snap-fit connectors, cable management clips, pneumatic fittings, and underhood automotive components. Mechanical data are normally published under ISO 527-1:2012, ISO 527-2:2012, ISO 179-1eA:2010, ISO 178:2019, and ISO 1183-1:2019. The conditioning state is not a trivial packaging label; it alters the amorphous phase mobility of the polyamide matrix and therefore changes modulus, impact response, and failure elongation.

    What Limits Ductility After Conditioning in a 30% Glass-Filled PA12?

    The conditioned tensile response of Grilamid LV-3H reflects two competing mechanisms. Moisture absorption plasticises the PA12 matrix, increasing chain mobility and reducing yield stress. However, the glass fibres do not plasticise, and their ends remain as stress concentrators. As a result, the conditioned tensile modulus declines from the dry value, while elongation at break improves only moderately. Manufacturer-reported typical dry tensile modulus for 30% glass-filled PA12 is in the range of 5,500 MPa to 6,000 MPa under ISO 527-1/-2; after conditioning to 23°C and 50% RH, the modulus typically falls into the 4,000 MPa to 4,600 MPa band. Tensile strength at break follows a similar downward shift, commonly from approximately 85 MPa dry to 60–65 MPa conditioned. The Charpy notched impact strength under ISO 179-1eA tends to remain stable or rise slightly after conditioning because the matrix absorbs more energy before crack initiation. Fibre orientation, gate placement, and weld-line location can produce larger property deviations than the dry-to-conditioned shift itself. In thin-wall mouldings with wall sections below 1.2 mm, fibre orientation parallel to flow dominates, and transverse tensile strength may fall by 25% to 40% compared with flow-direction values. Designers using LV-3H data should therefore treat the conditioned isotropic datasheet values as a matrix baseline, not as a substitute for orientation-sensitive finite element input.

    Mechanical Property Matrix Across Dry and Conditioned States

    The following table consolidates typical manufacturer technical datasheet values for Grilamid LV-3H at 23°C. Values are not specification limits and may shift with colour, regrind content, moisture exposure time, and moulding conditions. The dry values represent injection-moulded specimens tested shortly after desiccant storage to a residual moisture content below 0.10% by weight. Conditioned values represent specimens equilibrated under ISO 1110:2019 conditions.

    PropertyUnitTest standardDryConditioned
    Densityg/cm³ISO 1183-11.231.23
    Tensile modulusMPaISO 527-1/-25,8004,500
    Tensile strength at breakMPaISO 527-1/-28562
    Elongation at break%ISO 527-1/-247
    Flexural modulusMPaISO 178:20195,0003,800
    Charpy notched impact at 23°CkJ/m²ISO 179-1eA:201089

    The dry-to-conditioned modulus loss of roughly 20% to 25% is lower than the corresponding shift in PA66-GF30, which can lose 30% or more of its dry tensile modulus after moisture conditioning because of higher equilibrium water absorption. This lower hygroscopic sensitivity is one of the primary selection criteria for LV-3H in humid service environments where snap-fit retention force must remain predictable.

    On production lines equipped with reciprocating-screw injection moulding machines using general-purpose three-zone screws with L/D ratios from 20:1 to 25:1, the most common processing failure associated with LV-3H is splay caused by residual moisture. Although PA12 is less hygroscopic than PA6 or PA66, exposed pellet surfaces can still pick up sufficient atmospheric water in high-humidity plants to produce silver streaks and reduced weld-line strength. Desiccant hopper drying at 80°C for 4 h to 6 h to a residual moisture content below 0.10% is routinely specified, with a supply-air dew point of -30°C or lower. Pre-drying at relative humidity above 60% in an open container is not adequate. Regrind use above 20% introduces wider glass-fibre length distribution and can shift spiral flow length and impact data; production trials with the exact regrind fraction are required because published data for this specific configuration is limited. Barrel residence time should not exceed 10 min at melt temperature, and hot-runner dead spots should be avoided. Melt temperature is typically controlled between 220°C and 260°C, with mould temperature maintained between 40°C and 80°C. Higher mould temperatures improve surface finish and crystallinity but can extend cycle time. Mould temperature uniformity below ±5°C across the cavity is advisable for dimensional consistency in close-tolerance snap-fit geometries.

    Because conditioned PA12-GF30 retains a higher proportion of its dry stiffness under humid service than PA6-GF30 or PA66-GF30, LV-3H is used in underhood automotive clips, fuel-system retention brackets, cable harness clamps, pneumatic connectors, and sensor housings where hydrocarbon exposure and thermal cycling are present. The glass reinforcement provides the creep resistance needed for sustained clamping loads, while the PA12 matrix contributes low water absorption and resistance to automotive fuels, oils, greases, and aliphatic hydrocarbons. In fuel vapor management components, the material is evaluated using prolonged fuel immersion and heat ageing because PA12 can undergo oxidative embrittlement at elevated temperature if antioxidant packages are depleted. Continuous-use temperature limits must be established by heat ageing under ISO 188 or equivalent OEM test methods with a retained elongation criterion, not by a single HDT value. Zinc chloride resistance is a differentiation point against PA6 and PA66 in winter road-salt environments; PA12 grades show less stress-cracking sensitivity, although published comparative data under specific field conditions is limited. For parts exposed to hot water, glycol, or strong acids, the standard LV-3H grade is not recommended without component-level validation.

    When Dimensional Stability in Humid Load Paths Excludes PA66-GF30 Grades

    Moisture uptake at 23°C and 50% RH for PA12-GF30 is typically below 0.8% by weight, whereas PA66-GF30 commonly reaches 2.3% to 2.8% and PA6-GF30 can exceed 3% under the same exposure. At saturation, the difference widens further: PA12-GF30 may absorb approximately 1.5%, while PA66-GF30 can approach 8%. This lower water absorption translates into smaller dimensional growth, reduced modulus drop, and higher retention of snap-fit force in humid environments. In gears, clips, and connector bodies subject to seasonal humidity variation, PA66-GF30 parts can show enough hygroscopic swelling to alter mating clearances or increase insertion force. PA12-GF30 reduces that variation, but it does not eliminate it. Dimensional change from dry to conditioned still occurs at the level of a few tenths of a percent, so precision fits require moisture-conditional tolerancing. Against PA6-GF30, the PA12 backbone also provides lower density and better low-temperature impact behaviour, although PA6-GF30 tends to provide higher dry stiffness at equal glass loading. Against unreinforced PA12, LV-3H offers higher modulus, lower thermal expansion, and improved creep resistance, but sacrifices isotropy and ductility. For parts requiring maximum chemical resistance and electrical insulation rather than stiffness, an unfilled PA12 grade may be a more appropriate selection.

    For regulatory documentation, the standard Grilamid LV-3H grade is typically covered under EU RoHS Directive 2011/65/EU Annex II and REACH Regulation (EC) No 1907/2006 as reported on the supplier safety data sheet. WEEE Directive obligations may apply only to finished electrical and electronic equipment, not to the polymer raw material. If the application requires food-contact status, FDA 21 CFR or EU Regulation 10/2011 compliance must be confirmed for the specific pigment and lot because standard engineering grades are not automatically cleared for food-contact use. The material should not be combined with amine-based cleaning agents or strongly oxidizing process aids without verification of surface degradation or discolouration.

    Processing Window Boundaries and Production Floor Failure Signals

    Melt temperature for LV-3H is bounded by two failure modes. Below approximately 210°C, the melt viscosity rises rapidly and the risk of incomplete filling and excessive orientation in thin sections increases. Above 270°C, residence-time-dependent chain scission and oxidative yellowing become more probable, particularly at hot-runner valve gates or in machines with large shot capacity. Mould temperature below 40°C can produce a coarse surface, low crystallinity, and poor knit-line strength; above 80°C the part may require extended cooling and may stick to the core. Injection speed should be set to avoid excessive shear heating in gates smaller than 0.8 mm. Shear-induced fibre breakage in small gates can reduce tensile strength and impact performance. Weld lines in glass-filled PA12 are particularly sensitive: under ISO 527 testing of welded or knit-line specimens, strength retention relative to the bulk material can fall by 25% to 40% depending on glass fibre orientation at the meeting front. Mould-filling simulation with fibre orientation modelling is used to reposition knit lines away from snap-fit roots or other high-tensile locations. Dimensional checks should be performed after conditioning, not immediately after ejection, because PA12-GF30 continues to absorb moisture during storage and the resulting small expansion can shift hole-to-hole distances by more than the tolerance band in precision connectors.

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