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EcoVid 30GBIM General Purpose High Molecular Weight Ingeo PLA

    • Product Name: EcoVid 30GBIM General Purpose High Molecular Weight Ingeo PLA
    • Factroy Site: Yudu County, Ganzhou, Jiangxi, China
    • Price Inquiry: admin@ascent-chem.com
    • Manufacturer: Ascent Petrochem Holdings Co., Limited
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    Specifications
    HS Code 699893
    Product Name EcoVid 30GBIM General Purpose High Molecular Weight Ingeo PLA
    Brand EcoVid
    Manufacturer 3DXTECH
    Sku 30GBIM
    Material Polylactic Acid (PLA)
    Polymer Type Ingeo PLA
    Grade High Molecular Weight General Purpose
    Filament Diameter 3.00 mm
    Net Weight 1 kg
    Color Black
    Density 1.24 g/cm³
    Melt Flow Rate 7-9 g/10 min at 210 °C
    Glass Transition Temperature 55-60 °C
    Melting Temperature 165-180 °C
    Heat Deflection Temperature 55 °C at 0.45 MPa
    Vicat Softening Temperature 55 °C
    Tensile Strength 62 MPa
    Tensile Modulus 3.6 GPa
    Elongation At Break 6%
    Flexural Strength 108 MPa
    Flexural Modulus 3.8 GPa
    Notched Izod Impact Strength 2.6 kJ/m²

    As an accredited EcoVid 30GBIM General Purpose High Molecular Weight Ingeo PLA factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing EcoVid 30GBIM General Purpose High Molecular Weight Ingeo PLA is supplied in 25 kg moisture-barrier bags, palletized for shipping.
    Container Loading (20′ FCL) EcoVid 30GBIM General Purpose High Molecular Weight Ingeo PLA is palletized, shrink-wrapped, and securely loaded into a dry 20′ FCL container.
    Shipping EcoVid 30GBIM Ingeo PLA ships as a non-hazardous, non-regulated solid polymer in moisture-barrier bags, lined cartons, or bulk containers. Keep dry and cool, away from direct sunlight and excessive heat. Palletized loads are stable for truck, rail, sea, or air freight; no special transport placards required.
    Storage Store EcoVid 30GBIM Ingeo PLA in a cool, dry, well-ventilated area, away from heat, flames, and direct sunlight. Keep containers tightly closed to prevent moisture absorption and contamination. Use original packaging; avoid prolonged exposure to humid air. Maintain ambient temperatures below 30°C if possible, and rotate stock. Consult supplier SDS for detailed handling and shelf-life requirements.
    Shelf Life Shelf life is 24 months when stored unopened in a cool, dry place, away from moisture and direct sunlight.
    Application of EcoVid 30GBIM General Purpose High Molecular Weight Ingeo PLA

    Pre-drying of the 30GBIM resin to a residual moisture content below 250 ppm (0.025%) is the controlling operation before injection molding, because hydrolytic chain scission during plasticating occurs rapidly above this threshold and preferentially attacks the high-molecular-weight fraction that most contributes to melt strength. A closed-loop desiccant dryer with a -40 °C dew point and 80 °C inlet air usually reduces pellet moisture within 4 h; hopper residence beyond 6 h at 55 °C should be limited to avoid surface tack and pellet bridging. Melt temperature measured directly at the nozzle is maintained between 195 °C and 210 °C, with the lower third of the range preferred for thin-walled parts when the machine uses a heated sprue bushing and valve-gated hot runners. The reciprocating screw should have a 20:1 to 24:1 L/D ratio and a compression ratio of 2.5:1 to 3.0:1, while back pressure is set between 5 bar and 10 bar to avoid excessive shear heating without sacrificing melt homogeneity. Mold temperature is typically 15 °C to 25 °C for gloss and short cycle times, but the high-molecular-weight backbone reduces melt flow and can produce flow hesitation behind ribs thinner than 1.0 mm. Increasing mold temperature to 35 °C or using sequential valve gating resolves sink marks and weld-line visibility at the cost of cycle-time extension. Injection velocity should be profiled with a short fast-fill phase followed by a controlled packing threshold, because the high melt elasticity of the resin can otherwise create jetting streaks and gate blush.

    The resulting rigid articles include single-use cold-food containers, portion cups, clear deli lids, and disposable cutlery. These products are evaluated for industrial compostability under EN 13432:2000 or ASTM D6400-19, requiring aerobic biodegradation of at least 90% and disintegration within 12 weeks. Tensile properties of molded parts are typically measured per ISO 527-2 or ASTM D638-14, and notched impact strength per ISO 180 or ASTM D256-10. Annealed parts must be tested separately because crystallization raises heat deflection temperature but reduces impact toughness. The processing limitation is sharp: residence time at melt temperature above 230 °C beyond 5 min can trigger lactide reformation and surface oligomer bloom. Hot-runner channels must be sized without dead spots and purged before shutdown.

    Process parameterInjection moldingSheet extrusionFilament extrusion
    Pellet moisture target0.025% max0.025% max0.025% max
    Melt temperature195–210 °C200–215 °C200–210 °C
    Cooling medium setpoint15–25 °C mold25–50 °C roll stack40–50 °C water bath
    L/D ratio20:1–24:124:1–30:120:1–24:1 plus melt pump
    Critical control limitresidence <5 min above 230 °Cthickness variance ±0.05 mmmelt-pressure ripple <0.5%

    When Does Sheet Thickness Variability Override the Forming Window?

    30GBIM sheet is usually extruded at melt temperatures between 200 °C and 215 °C through a coat-hanger or flexible-lip flat die with die gap set at 0.8 to 1.0 times final gauge. A three-roll stack with polished rolls commonly operates at 25 °C top, 40 °C middle, and 50 °C bottom to control surface texture and sag. Because the grade’s high molecular weight produces pronounced shear thinning, thickness variation above ±0.05 mm across the web can shift the thermoforming window by more than 5 °C. Zones that are too thin overstretch and whiten under plug-assist pressure, while zones that are too thick retain excessive orientation and cause warpage after trimming. Sheet gauge consistency is therefore more critical for this resin than for a low-viscosity PLA, particularly when forming depth exceeds 30 mm.

    Thermoforming is performed at sheet surface temperature between 90 °C and 115 °C, measured with infrared pyrometry immediately before plug-assist activation. The plug should be heated to 80 °C to 100 °C and advanced with controlled delay to avoid premature crystallization haze. Mold temperature is held between 25 °C and 40 °C; lower mold temperatures improve cycle time but can freeze surface defects. Trim scrap is dry-ground and reintroduced at up to 30 wt%. Higher regrind fractions reduce intrinsic viscosity below the point where sag resistance during heating is lost, especially when scrap has been exposed to moisture above 0.05%. Each additional extrusion cycle at 200 °C reduces molar mass through thermal and hydrolytic degradation, although published data for this specific configuration is limited. End products include deli lids, produce trays, blister inserts, and cold-serve packaging. Puncture resistance is measured according to ISO 6603-2:2000, and industrial compostability is verified under EN 13432:2000.

    For filament production from 30GBIM, a single-screw extruder with a melt pump and gear-driven melt filtration is required because melt-pressure fluctuations above 0.5% translate directly into diameter drift outside the ±0.05 mm tolerance expected by printing hardware. Pellets are dried to 0.025% moisture or lower, then melted at 200 °C to 210 °C through a 60/100/60 mesh screen pack to remove gel particles and pigment agglomerates. The molten strand enters a water bath held at 40 °C to 50 °C; lower bath temperatures produce oversized, oval filaments because the high molecular weight delays solidification and permits die swell. A dual-axis laser gauge downstream of the cooling bath feeds an error signal to a capstan puller that maintains tension between 0.5 N and 1.5 N. Excessive tension introduces internal stress that later manifests as warped printed parts. Color concentrates with PLA carrier are added at 1 to 3 wt%, with the carrier melt-flow rate selected within 5 g/10 min of the base resin to avoid diameter oscillations.

    During printing, the filament is extruded through a 0.4 mm brass or hardened steel nozzle at 210 °C to 225 °C, with bed temperature between 50 °C and 60 °C on glass or PEI sheets. The high molecular weight raises melt pressure but improves interlayer adhesion when the extrusion multiplier is reduced by 2 to 5%; overextrusion causes nozzle chatter and dimensional inaccuracy. Tensile data generated per ASTM D638-14 or ISO 527-2 are meaningful only after conditioning at 23 °C and 50% RH for 48 h per ISO 291:2008. Output parts are prototype housings, educational tooling, and low-temperature jigs, not continuous-use load-bearing components, because the heat deflection temperature of unannealed PLA remains below 55 °C at 0.455 MPa load per ISO 75-2:2013. The operational boundary excludes high-humidity service above 60% RH without sealing or annealing.

    Meltblown Die Tip Accumulation and Low-MFI Resin Limitations

    In meltblown equipment rated for fine-fiber output, high-molecular-weight general-purpose PLA of the 30GBIM class is not an optimized resin. Its melt-flow index, typically below 10 g/10 min at 210 °C under 2.16 kg load per ISO 1133-1:2022, restricts fiber attenuation from single-row die tips with 0.25 mm orifice diameter and 35 to 40 holes per inch. At melt temperatures below 230 °C, elongational viscosity remains too high for fine-fiber formation, while above 240 °C molecular weight reduction broadens the fiber diameter distribution. Published data for this specific configuration is limited; most commercial PLA meltblown systems use low-viscosity grades with MFR values above 60 g/10 min under the same conditions. Quench air should be dried to a dew point below -20 °C to reduce condensation and oligomer deposit formation on the die face.

    If a nonwoven line is nevertheless used, the extruder should be configured with L/D of 30:1 or higher and a melt pump to stabilize throughput below 10 kg/h/m of die width. Collector belt distance is set between 150 mm and 300 mm to allow fiber solidification; shorter distances produce fused film-like structures due to incomplete cooling. End products are limited to stiff scrim layers, acoustic insulation mats, or compostable hygiene packaging where fiber diameter uniformity is not critical. Medical filtration markets are excluded unless the material passes ISO 10993-5 cytotoxicity screening and the specific nonwoven structure meets EN 14683 sub-micron filtration efficiency requirements. The general-purpose resin does not provide the consistent sub-micron fiber population required for high-efficiency filtration without aggressive viscosity modification.

    If Chemical Blowing Agent Decomposition Is Mismatched to Melt Temperature

    When closed-cell foam is extruded from 30GBIM, the onset decomposition temperature of the endothermic blowing agent must match the melt temperature at the die exit. Citric acid–bicarbonate systems that release CO₂ between 150 °C and 210 °C are typically applied at 0.5 to 2.0 wt%, while talc nucleation is introduced at 0.1 to 0.5 wt% to reduce cell size. If melt temperature exceeds 215 °C before the die exit, premature gas evolution inside the screw generates surging and non-uniform density; below 185 °C, undecomposed particles remain in the structure and act as defects that lower compressive strength. The high-molecular-weight backbone provides more melt strength than a low-viscosity, high-MFR PLA grade, but it is not equivalent to a high-melt-strength branched grade. Density reduction is therefore usually limited to 0.6 g/cm³ to 0.8 g/cm³ without cell collapse.

    Physical foaming with CO₂ or N₂ requires gas delivery and static mixers capable of 2 to 5 wt% gas loading, with melt pressure maintained above 80 bar throughout the melt stream. The foam is calendered or conveyed through a shaping die into trays, blocks, or sheet for protective packaging. Compressive stress at 10% strain is measured per ISO 844:2014, density per ISO 1183-1:2019, and closed-cell content per ASTM D6226-21. The operational boundary is severe: any moisture above 0.05% in the melt promotes hydrolysis and causes pinholes at the foam surface. Chemical foaming concentrates, nucleating agents, and regrind must all be dried with the base resin to prevent batch-to-batch density drift.

    Barrier Film Oxygen Transmission after Orientation, Not Just Moisture

    Before orientation at a draw ratio above 2.0:1, cast film produced from 30GBIM is extruded through a flat die at 200 °C to 215 °C, chilled on a 15 °C to 25 °C polished roll, and optionally stretched in the machine direction at draw ratios between 2.0:1 and 3.0:1. Unoriented PLA film at 25 µm thickness has oxygen transmission rates near 400 cm³/(m²·day·bar) at 23 °C and 0% RH per ASTM D3985-17; orientation lowers this value but also reduces elongation at break measured per ISO 527-3:2018. The film’s seal initiation temperature is recorded by hot-tack testing under ASTM F1921-12, with target values usually falling between 80 °C and 100 °C depending on D-lactide content and sheet crystallinity. Corona treatment at 1.5 to 2.5 kW output increases surface energy above 40 mN/m for lamination or water-based ink adhesion. Slip and antiblock masterbatches are added at 0.5 to 1.0 wt% to prevent blocking during winding and unwinding.

    Applications include compostable labels, window films, fresh-produce flow-wrap, and cold-seal release liners. Compliance with EN 13432:2000 requires disintegration in a composting environment within 12 weeks, while food-contact migration limits follow EU Regulation 10/2011, with overall migration below 10 mg/dm² for the final article. The operational incompatibility is with high-fat or hot-fill contents; migration and mechanical stability under those conditions require additive modification and are outside the general-purpose specification. Moisture barrier is not comparable to polyethylene or polypropylene, and ASTM F1249-20 water vapour transmission data must be reviewed for the target shelf-life before film replacement.

    Regulatory/technical referenceScopeTypical acceptance criterion
    EN 13432:2000Compostable packaging recovery≥90% biodegradation in 180 days; disintegration 12 weeks
    ASTM D6400-19US industrial compostability≥90% mineralization over 180 days
    EU Regulation 10/2011Plastic food-contact materialsoverall migration 10 mg/dm²
    ISO 527-3:2018Tensile properties of filmmeasured after 48 h at 23 °C/50% RH
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    Certification & Compliance
    More Introduction

    EcoVid 30GBIM General Purpose High Molecular Weight Ingeo PLA is an unfilled polylactide resin specified for general-purpose extrusion and injection molding operations where melt strength and molecular weight retention are the limiting variables. The product designation places it in the high-molecular-weight portion of the Ingeo PLA family, with a lower melt flow rate than standard general-purpose injection grades. Because a product-specific public datasheet for this model is not available, the technical boundaries in this discussion are drawn from high-molecular-weight Ingeo PLA reference data and should be confirmed against the supplier lot certificate. Comparable high-MW Ingeo PLA resins typically exhibit a melt flow rate of 2–10 g/10 min at 210 °C under 2.16 kg load when tested according to ISO 1133-1:2022. Solid density is generally 1.24 g/cm³ under ISO 1183-1:2019. The resin is neither a high-flow thin-wall injection grade nor an impact-modified ductile PLA; its differentiation lies in higher extensional viscosity, reduced edge neck-in during cast film processing, and greater tolerance for melt-phase drawing operations.

    In production-scale cast film and sheet operations, high-molecular-weight PLA resins are used when edge neck-in, bubble sag, or draw resonance limit line speed. On three-layer cast film dies with lip gaps of 0.4–0.8 mm, the 30GBIM molecular architecture is expected to provide extensional viscosity above that of low-viscosity Ingeo PLA. Single-screw extruders with grooved feed sections and L/D ratios between 24:1 and 30:1 should be fed with positive displacement rather than flood feeding to prevent screw slip and melt-pressure oscillation. Barrel temperature set points from 170 °C at the feed zone to 210 °C at the metering zone, with a die temperature of 195 °C, are commonly used starting references for high-MW PLA. Melt temperature should not exceed 240 °C because poly(L-lactide) thermal degradation proceeds through unzipping and random chain scission; lactide vapor appears as condensate on vacuum vents. Published data for this specific 30GBIM configuration is limited, so initial production trials should include rheological characterization of the as-received pellets and a purge protocol using lower-viscosity PLA at 200 °C to remove shear-degraded boundary layers from the die land.

    What Moisture Uptake Limits Are Relevant Before Melt Processing?

    Ingeo PLA resins are hygroscopic and undergo melt-state hydrolysis at free moisture above 250 ppm. Drying in a desiccant-bed dryer at 80 °C for 4 h is required when ambient relative humidity exceeds 60%; the drying air dew point should be at or below −40 °C. Residual moisture is measured by Karl Fischer titration or by a moisture analyzer following ISO 15512:2019. On twin-screw extruders with L/D 30:1 operating from 180 °C to 210 °C, insufficient drying produces gas bubbles in extruded strand, melt-pressure fluctuation, and tensile strength losses of 10–20% after pelletizing. Once dried, pellets rehydrate rapidly: at 25 °C and 50% RH, surface moisture can return to process-significant levels within 15–30 min. Dried material must therefore be conveyed under dry air and held in hoppers purged to a dew point no higher than −30 °C. Long drying times above 4 h at 80 °C do not appreciably improve viscosity and may increase yellowness if oxygen is not excluded.

    Melt-phase rheology is characterized by a shear-thinning power-law index between 0.4 and 0.6 across shear rates from 10 s⁻¹ to 1000 s⁻¹ at 200 °C. The apparent shear viscosity at 100 s⁻¹ for high-MW Ingeo PLA typically falls between 200 Pa·s and 600 Pa·s at 200 °C. Melt strength measured on a Rosand capillary rheometer with a haul-off attachment is commonly in the range of 0.05–0.15 N at 190 °C, compared with 0.02–0.06 N for low-viscosity injection PLA. These rheological differences explain why gate freeze time, nozzle pressure drop, and cooling time are longer than for low-viscosity grades. Injection molding with high-MW PLA requires back pressure of 0.5–1.5 MPa, screw rotation speed of 50–150 rpm, and a clamp force of 3–5 kN/cm² of projected area. Cooling time may need to be extended by 10–15% relative to standard PLA in thin-wall tools. The material should not be held above 220 °C for more than 5 min; residence time beyond this threshold produces measurable molecular weight loss by chain scission and lactide regeneration, even if visual degradation is not yet apparent.

    Cold-runner molds with hardened S136 or P20 steel cavities are used. The high molecular weight increases melt viscosity at the gate, so gate diameters below 0.8 mm may cause jetting unless the injection velocity is reduced. Mold temperature uniformity should be held within ±2 °C across the cavity to avoid differential shrinkage and sink marks. PLA has a high affinity for polished steel; release difficulty appears when the mold temperature exceeds 40 °C because the part remains soft during ejection.

    Thermo-Mechanical Performance Under Static Tensile and Flexural Loading

    Unfilled high-molecular-weight Ingeo PLA exhibits tensile yield stress in the band of 55–65 MPa when tested to ISO 527-2:2012 on injection-molded type 1A specimens. Tensile modulus is commonly 3.2–3.6 GPa, flexural modulus 3.0–3.5 GPa under ISO 178:2019, and strain at break remains at 2–5%. Notched Izod impact values for unfilled high-MW PLA are generally 20–30 J/m under ASTM D256-23; the molecular weight increase provides only marginal toughening because the polymer remains brittle in the glassy state. The primary mechanical benefit is a reduction in flow-induced defects and better melt-state strength retention, not ductile failure. In applications involving repeated drop impact, hinge bending, or sub-zero service, an impact-modified PLA should be selected instead. Tensile bars conditioned at 23 °C and 50% RH for 48 h show tensile strength reductions of less than 5% compared with dry-as-molded values, but conditioning above 80% RH can produce larger losses through hydrolysis of the amorphous phase.

    For systematic grade selection across the Ingeo PLA family, the following reference bands are generalized from publicly available technical literature. They are not lot-specific certificates for EcoVid 30GBIM and must be confirmed against the actual material specification.

    PropertyTest method30GBIM high-MW reference bandLow-viscosity injection PLAImpact-modified PLA
    Melt flow rate at 210 °C/2.16 kgISO 1133-1:20222–10 g/10 min15–40 g/10 min10–30 g/10 min
    Tensile yield stressISO 527-2:201255–65 MPa50–60 MPa35–45 MPa
    Strain at breakISO 527-2:20122–5%2–4%10–30%
    Notched Izod impactASTM D256-2320–30 J/m15–25 J/m60–150 J/m
    HDT at 0.455 MPa, amorphousISO 75-2:201350–55 °C50–55 °C45–50 °C

    When Heat Deflection and Crystallization Behaviour Govern Process Cycle Time

    Amorphous PLA heat deflection temperature under 0.455 MPa load is typically 50–55 °C when tested to ISO 75-2:2013. The high-molecular-weight grade retains this thermal limitation unless crystallinity is deliberately induced by mold temperatures above 90 °C, by nucleating agents, or by post-mold annealing at 100 °C for 30 min. Differential scanning calorimetry at 10 °C/min shows a cold crystallization exotherm near 100–120 °C and a melting endotherm near 155–170 °C; annealed samples can reach 30–40% crystallinity. Isothermal crystallization half-times are strongly temperature-dependent: at 110 °C, a nucleated PLA can reach a half-time below 1 min, while at 90 °C the half-time often exceeds 5 min. Non-isothermal cooling above 20 °C/min suppresses crystallization almost entirely. Therefore, hot-mold cycle-time optimization requires a mold temperature of at least 100 °C and sufficient hold pressure to compensate for crystallization shrinkage. Mold shrinkage in the flow direction for amorphous parts is approximately 0.3–0.5%, while annealed semicrystalline parts can reach 1.0–1.5%. Processors should not combine 30GBIM with amine-based additives or polyamides with amine end groups; these catalyze chain scission in the melt and shift the melt flow rate outside the high-MW processing band.

    Monofilament extrusion for fused filament fabrication uses a single-screw extruder with L/D 24:1–30:1, a water-bath quench at 20–40 °C, and laser micrometer control of diameter to ±0.03 mm. The high molecular weight provides the die swell and melt strength required for roundness retention at a draw ratio of 1.5:1 to 2.5:1, with the cooling bath placed 50–100 mm from the die. Exceeding these draw ratios produces ovality and surface stress whitening. On production lines, diameter variation is more often traced to inconsistent pellet feeding, wet resin, or insufficient melt-temperature uniformity than to molecular weight variation in the supplied lot. Batch-to-batch melt flow rate variation for commercial Ingeo PLA is typically less than ±1.0 g/10 min, but regrind content and drying history can shift viscosity more than intrinsic lot variation.

    In masterbatch dilution, the shear-degraded boundary layers on the die land can generate black specks after a high-MW resin has been held at 210 °C for extended periods. To prevent this, the die should be purged with a lower-viscosity PLA at 200 °C before shutdown, and the screw should be run at low speed to pull the degraded layer from the barrel wall. The resin is incompatible with acidic or basic additives that accelerate ester hydrolysis; neutral masterbatches with mineral fillers may require a coupling agent to prevent viscosity reduction and plate-out on molding tools.

    For food-contact applications, compliance must be confirmed for the complete formulation, including processing aids. In the European Union, unmodified Ingeo PLA grades are typically evaluated under EU 10/2011 for overall migration in simulant A (10% ethanol), simulant B (3% acetic acid), and simulant D2 (vegetable oil); the overall migration limit is 10 mg/dm². In the United States, food-contact use of polylactide is subject to the general provisions of 21 CFR 175.300 or an applicable Food Contact Notification, and the specific Ingeo grade should be listed by the supplier for the intended use. Compostability is not established by the polylactide backbone alone; finished articles require separate testing to EN 13432 or ASTM D6400. RoHS screening for cadmium, lead, mercury, and hexavalent chromium is performed by IEC 62321-5:2013; unmodified PLA is expected to yield results below detection limits. The resin should be stored in sealed foil-lined containers at 10–30 °C and below 50% RH. Opened containers should be consumed within 8 h unless connected to a dry-air purge. Avoid combination with amine-based additives and sustained hold times above 220 °C. The processing boundaries described here are drawn from the Ingeo PLA family; a formulation-specific technical data sheet from the supplier remains the authoritative source for lot-specific release limits.

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